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zcy881223金蟲(chóng) (正式寫(xiě)手)
科學(xué)家
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[求助]
單晶衍射模擬的XRD峰與粉末位置一致,強(qiáng)度差異較大!怎么解決
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現(xiàn)在審稿人非卡住這個(gè)問(wèn)題不放,請(qǐng)問(wèn)大神該怎么解決,如能解決,可以花錢(qián)。 The PXRD patterns shown in the supplement suggest that both samples are not phase pure. I am not convinced by the authors only arguing that the reason might be a preferential orientation without presenting any conrmation of this fact, may- be by a Rietveld renement or an accordingly calculated diraction pattern. Mo- reover, still no sucient experimental details are given like sample geometry or recording times. Please add. The authors should note, that if the samples were not phase pure, then all physical property measurements are meaningless. |

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金蟲(chóng) (正式寫(xiě)手)
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新蟲(chóng) (正式寫(xiě)手)
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樓主別嚇我啊 一般我們都只看了出峰位置是否吻合,強(qiáng)度這個(gè)因素太多怎么能要求強(qiáng)度也一致呢 同等大神回復(fù) 發(fā)自小木蟲(chóng)Android客戶端 |
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