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maqing4399木蟲 (正式寫手)
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[求助]
求解單晶,數(shù)據(jù)很好,就是解不出來,求高手 已有2人參與
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| 主要是CHNO,不排除Na,K,Cl,Br,S等元素 |
木蟲 (正式寫手)
木蟲 (正式寫手)
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禁蟲 (著名寫手)
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本帖內(nèi)容被屏蔽 |
禁蟲 (著名寫手)
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木蟲 (正式寫手)
| http://pan.baidu.com/s/1sjutsC1大概就這樣,但是有個A類錯誤,我沒辦法,希望論壇里的高手伸出援手。 |
鐵桿木蟲 (著名寫手)
捐助貴賓 (著名寫手)
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在7樓的基礎(chǔ)上精修了一下,那個原子不是Cl,而是K。 Bond precision: C-C = 0.0040 A Wavelength=0.71073 Cell: a=7.6179(3) b=7.6179(3) c=13.3498(5) alpha=90 beta=90 gamma=120 Temperature: 293 K Calculated Reported Volume 670.93(7) 670.93(4) Space group P 31 2 1 P3121 Hall group P 31 2" ? Moiety formula C3 H2 K2 N4 O8 ? Sum formula C3 H2 K2 N4 O8 C3 H2 K2 N4 O8 Mr 300.29 300.29 Dx,g cm-3 2.230 2.230 Z 3 3 Mu (mm-1) 1.106 1.106 F000 450.0 450.0 F000' 451.47 h,k,lmax 9,9,15 9,8,15 Nref 788[ 486] 791 Tmin,Tmax 0.784,0.838 0.793,0.843 Tmin' 0.784 Correction method= # Reported T Limits: Tmin=0.793 Tmax=0.843 AbsCorr = MULTI-SCAN Data completeness= 1.63/1.00 Theta(max)= 24.970 R(reflections)= 0.0308( 751) wR2(reflections)= 0.0630( 791) S = 1.063 Npar= 78 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT090_ALERT_3_C Poor Data / Parameter Ratio (Zmax > 18) ........ 6.23 Note Alert level G PLAT004_ALERT_5_G Polymeric Structure Found with Maximum Dimension 3 Info PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! |
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