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終結(jié)者925銅蟲 (正式寫手)
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[求助]
晶體精修出現(xiàn)很多A類錯(cuò)誤,請(qǐng)指導(dǎo)怎么解決,謝謝 已有1人參與
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SYMM001_ALERT_1_A _symmetry_cell_setting is missing The cell setting should be one of the following * triclinic * monoclinic * orthorhombic * tetragonal * rhombohedral * trigonal * hexagonal * cubic The following tests will not be performed. SYMMS_01,SYMMS_02 EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. SHFSU01_ALERT_2_A The absolute value of parameter shift to su ratio > 0.20 Absolute value of the parameter shift to su ratio given 3.681 Additional refinement cycles may be required. PLAT043_ALERT_1_A Calculated and Reported Mol. Weight Differ by .. 853.58 Check PLAT051_ALERT_1_A Mu(calc) and Mu(CIF) Ratio Differs from 1.0 by . 80.22 % PLAT080_ALERT_2_A Maximum Shift/Error ............................ 3.68 Why ? PLAT122_ALERT_1_A No _symmetry_space_group_name_H-M Given ........ Please Do ! PLAT211_ALERT_2_A ADP of Atom O1 is N.P.D. or (nearly) 2D ... Please Check And 9 other PLAT211 Alerts More ...PLAT213_ALERT_2_A Atom N26 has ADP max/min Ratio ..... 5.5 prolat And 5 other PLAT213 Alerts Less ... PLAT213_ALERT_2_A Atom C14 has ADP max/min Ratio ..... 6.5 prolat PLAT213_ALERT_2_A Atom C30 has ADP max/min Ratio ..... 9.4 oblate PLAT213_ALERT_2_A Atom C40 has ADP max/min Ratio ..... 5.4 prolat PLAT213_ALERT_2_A Atom C71 has ADP max/min Ratio ..... 6.1 prolat PLAT213_ALERT_2_A Atom C75 has ADP max/min Ratio ..... 5.7 oblate PLAT214_ALERT_2_A Atom F20 (Anion/Solvent) ADP max/min Ratio 9.0 oblate PLAT353_ALERT_3_A Long N-H (N0.87,N1.01A) N38 - H13_a .. 1.41 Ang. PLAT431_ALERT_2_A Short Inter HL..A Contact F22 .. N38 .. 2.20 Ang. PLAT431_ALERT_2_A Short Inter HL..A Contact F24 .. N38 .. 2.30 Ang. |
專家顧問 (文壇精英)
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專家經(jīng)驗(yàn): +1066 |
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前兩三個(gè)都好解決,是因?yàn)镃IF文件缺失相關(guān)信息,填上就好,后幾個(gè)是晶體精修的問題,建議你找個(gè)明白人弄一下 發(fā)自小木蟲Android客戶端 |

銅蟲 (正式寫手)
專家顧問 (文壇精英)
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專家經(jīng)驗(yàn): +1066 |

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