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作者：Haiyan Kang, Yanli Mao, Xianli Wang, Yan Zhang, Junfeng Wu, Hongqiang Wang. 題目：Disposable ionic liquid-coated etched stainless steel fiber for headspace solid-phase microextraction of organophosphorus flame retardants from water samples, 期刊：RSC Adv., 年卷期頁碼：2015, 5,41934-41940 |
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Disposable ionic liquid-coated etched stainless steel fiber for headspace solid-phase microextraction of organophosphorus flame retardants from water samples 作者:Kang, HY (Kang, Haiyan)[ 1 ] ; Mao, YL (Mao, Yanli)[ 1 ] ; Wang, XL (Wang, Xianli)[ 1 ] ; Zhang, Y (Zhang, Yan)[ 1 ] ; Wu, JF (Wu, Junfeng)[ 1 ] ; Wang, HQ (Wang, Hongqiang)[ 1 ] RSC ADVANCES 卷: 5 期: 52 頁: 41934-41940 DOI: 10.1039/c5ra03504j 出版年: 2015 查看期刊信息 摘要 A simple and sensitive method for determining organophosphorus flame retardants (PFRs) in water samples was first developed based on headspace solid-phase microextraction (HS-SPME) using an ionic liquid-coated etched stainless steel (IL-ESS) fiber followed by a gas chromatography-flame photometric detector (GC-FPD). The etched stainless steel wire, whose rough and porous structure could not only allow IL to be held properly but also load more IL, was used as the support of the prepared fiber. The experimental results proved that the extraction capacity of the proposed fiber was higher than that of other conventional disposable IL-based coatings and the commercial SPME fibers. Parameters affecting the extraction efficiency were investigated. Under the optimal extraction conditions, the linear range of the proposed method was in the range of 10-5 x 10(4) ng L-1. The reproducibility of fiber-to-fiber (n = 6) was in the range of 3.9-8.2%. The method detection limits (signal/noise = 3) were in the range of 0.8-9.3 ng L-1. The proposed method was successfully applied to the determination of PFRs in the real water samples with good recoveries (78.2-105.8%) and low relative standard deviations (less than 7.7%). The results demonstrate that the proposed method was very attractive for the analysis of PFRs in water. 關(guān)鍵詞 KeyWords Plus:CHROMATOGRAPHY-MASS SPECTROMETRY; WALLED CARBON NANOTUBES; SURFACE WATERS; PHOTOMETRIC DETECTOR; ENVIRONMENTAL WATER; PHTHALATE-ESTERS; WASTE-WATER; PLASTICIZERS; EXTRACTION; WIRE 作者信息 通訊作者地址: Wang, XL (通訊作者) Henan Univ Urban Construct, Sch Municipal & Environm Engn, Pingdingshan 467036, Peoples R China. 地址: [ 1 ] Henan Univ Urban Construct, Sch Municipal & Environm Engn, Pingdingshan 467036, Peoples R China 電子郵件地址:wangxianli1223@163.com 基金資助致謝 基金資助機(jī)構(gòu) 授權(quán)號 National Natural Science Foundation of China 51108447 查看基金資助信息 出版商 ROYAL SOC CHEMISTRY, THOMAS GRAHAM HOUSE, SCIENCE PARK, MILTON RD, CAMBRIDGE CB4 0WF, CAMBS, ENGLAND 類別 / 分類 研究方向:Chemistry Web of Science 類別:Chemistry, Multidisciplinary 文獻(xiàn)信息 文獻(xiàn)類型:Article 語種:English 入藏號: WOS:000354445900073 ISSN: 2046-2069 |
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