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123/wq銅蟲 (初入文壇)
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[求助]
兩個(gè)晶體
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| 請(qǐng)求哪位大神幫幫忙解一下這兩個(gè)晶體,本人實(shí)在不會(huì)解,晶體的配體我都寫到壓縮包里了,是以wq命名的,如果能夠解好,本人將灰常感謝。! |
銅蟲 (初入文壇)
捐助貴賓 (著名寫手)
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兩個(gè)結(jié)構(gòu)都是很簡(jiǎn)單的零維結(jié)構(gòu),同構(gòu)的。 Bond precision: C-C = 0.0046 A Wavelength=0.71073 Cell: a=7.3183(13) b=9.1715(16) c=13.265(2) alpha=97.873(2) beta=103.665(2) gamma=110.526(2) Temperature: 293 K Calculated Reported Volume 786.2(2) 786.2(2) Space group P -1 P-1 Hall group -P 1 ? Moiety formula C26 H22 N4 O10 Zn, 2(C2 H3 N) ? Sum formula C30 H28 N6 O10 Zn C30 H28 N6 O10 Zn Mr 697.97 697.97 Dx,g cm-3 1.474 1.474 Z 1 1 Mu (mm-1) 0.848 0.848 F000 360.0 360.0 F000' 360.45 h,k,lmax 9,11,17 9,11,17 Nref 3592 3455 Tmin,Tmax 0.830,0.858 0.835,0.862 Tmin' 0.830 Correction method= # Reported T Limits: Tmin=0.835 Tmax=0.862 AbsCorr = MULTI-SCAN Data completeness= 0.962 Theta(max)= 27.410 R(reflections)= 0.0479( 3082) wR2(reflections)= 0.1479( 3455) S = 1.087 Npar= 223 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.962 Note PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C14 Check |
銅蟲 (初入文壇)
銅蟲 (初入文壇)
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