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q565090750金蟲 (小有名氣)
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[求助]
求大神幫忙修個結(jié)構(gòu),急需,要畢業(yè),幫幫忙 已有2人參與
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求大神幫忙修個結(jié)構(gòu),急需,要畢業(yè),幫幫忙 數(shù)據(jù):http://pan.baidu.com/s/1eQvywSy,求大神們幫幫忙,急需,要這個畢業(yè) |
捐助貴賓 (著名寫手)
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Bond precision: C-C = 0.0165 A Wavelength=0.71073 Cell: a=11.8356(7) b=11.8356(7) c=6.6317(8) alpha=90 beta=90 gamma=90 Temperature: 296 K Calculated Reported Volume 928.98(16) 928.98(14) Space group P 4/n P4/n Hall group -P 4a ? Moiety formula C16 H24 Cl N8 Na O4 Tb ? Sum formula C16 H24 Cl N8 Na O4 Tb C16 H24 Cl N8 Na O4 Tb Mr 609.80 609.79 Dx,g cm-3 2.180 2.180 Z 2 2 Mu (mm-1) 4.022 4.022 F000 602.0 602.0 F000' 602.18 h,k,lmax 15,15,8 15,15,8 Nref 1077 1068 Tmin,Tmax 0.429,0.485 0.472,0.531 Tmin' 0.397 Correction method= # Reported T Limits: Tmin=0.472 Tmax=0.531 AbsCorr = MULTI-SCAN Data completeness= 0.992 Theta(max)= 27.510 R(reflections)= 0.0668( 1044) wR2(reflections)= 0.1696( 1068) S = 1.184 Npar= 72 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT303_ALERT_2_C Full Occupancy H-Atom H3A with # Connections 2.00 Check PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0165 Ang. Alert level G PLAT004_ALERT_5_G Polymeric Structure Found with Maximum Dimension 3 Info PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 43.58 Why ? PLAT093_ALERT_1_G No su's on H-positions, refinement reported as . mixed Check |
木蟲 (正式寫手)
金蟲 (小有名氣)
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