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Bond precision: C-C = 0.0145 A Wavelength=0.71073 Cell: a=14.450(3) b=20.522(4) c=10.2395(18) alpha=90 beta=90 gamma=90 Temperature: 566 K Calculated Reported Volume 3036.5(10) 3036.4(10) Space group P 21 21 21 P212121 Hall group P 2ac 2ab ? Moiety formula C37 H34 N4 Ni O2 ? Sum formula C37 H34 N4 Ni O2 C37 H34 N4 Ni O2 Mr 625.37 625.39 Dx,g cm-3 1.368 1.368 Z 4 4 Mu (mm-1) 0.680 0.680 F000 1312.0 1312.0 F000' 1313.77 h,k,lmax 17,24,12 16,24,12 Nref 5338[ 3019] 4671 Tmin,Tmax 0.867,0.879 0.870,0.882 Tmin' 0.867 Correction method= # Reported T Limits: Tmin=0.870 Tmax=0.882 AbsCorr = MULTI-SCAN Data completeness= 1.55/0.88 Theta(max)= 25.000 R(reflections)= 0.1082( 4111) wR2(reflections)= 0.3271( 4671) S = 1.085 Npar= 398 -------------------------------------------------------------------------------- The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. --------------------------------------------------------------------------------Alert level C DIFMN02_ALERT_2_C The minimum difference density is < - |
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