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xuxiaodai鐵桿木蟲(chóng) (職業(yè)作家)
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[求助]
審稿人讓我測(cè)CO2或者Ar吸附,不是很理解這倆測(cè)試的作用,求幫助 已有1人參與
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審稿意見(jiàn)如下: On page 10, (starting in line 48) you ascribe the higher surface area as contribution of mesopores. This might be, but figure 6 also shows the highest amount of pores in the transition area of mesopores to micropores. However, you also have to consider the total amount of these micropores and compare these results with the evolution of mesopores. By skipping this comparison a clear statement is not possible. We would suggest to deliver further measurements in order to calculate the amount of micropores,e.g., by CO2 or Ar adsorption and to include a more detailed discussion on your results. 求大神指導(dǎo)。有人做過(guò)CO2或者Ar吸附?jīng)]?這些測(cè)試能得到哪些信息? |
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就是測(cè)BET吧,吸附質(zhì)換成氬氣。一般用氮?dú),由于氬氣比氮(dú)飧,極性也小,更容易進(jìn)入孔內(nèi),可能測(cè)試的結(jié)果也更好!對(duì)于介孔兩者差別不大,微孔可能相差稍大。 發(fā)自小木蟲(chóng)Android客戶(hù)端 |

木蟲(chóng) (正式寫(xiě)手)

鐵桿木蟲(chóng) (職業(yè)作家)
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