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summiler_XU銀蟲 (正式寫手)
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[求助]
投稿Talanta,審稿人意見如下,感覺遇到了統(tǒng)計學(xué)專家,求大神幫忙梳理一下,非常感謝 已有2人參與
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Reviewer #3: The ms is well written and organized. Especially Introduction and Experimental sections. The synthesis of the composite is well described and documented, though elemental analysis of the magnetic core (Fe3O4) was not provided. I am not convinced that it does not contain some residual water. In analytical part, it would far much better if authors could perform statistical analysis of the designed extraction experiment so that the optimal experimental conditions could by uniquely determined. Was it possible to compare obtained extraction yields with a standard method which produces known yields? Validation procedure should be performed more comprehensively. Linear parameters should be given with proper statistical ANOVA analysis and regression coefficients must be given with appropriate errors. LOD should be determined from the regression data and for S/N method data should be provided together with the significance test. A chromatogram of the synthetic mixture should be given together with the chromatogram of the extracted material from the real sample. |

銀蟲 (正式寫手)

金蟲 (著名寫手)
專家顧問 (正式寫手)
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專家經(jīng)驗: +179 |
專家顧問 (正式寫手)
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專家經(jīng)驗: +179 |
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1. 補(bǔ)充Fe3O4元素分析結(jié)果,確定是否含有結(jié)晶水 2. 運用化學(xué)計量學(xué)對萃取實驗進(jìn)行析因設(shè)計試驗 3. 與現(xiàn)有的已知萃取率的方法進(jìn)行對比,考察所建方法的萃取率 4. 補(bǔ)充方法確認(rèn)參數(shù),線性、回歸系數(shù)、回歸結(jié)果的誤差、檢出限、信噪比等 5. 補(bǔ)充合成的混合液(估計是模擬樣品)的色譜圖 |
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