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lo@丹丹@ve金蟲(chóng) (小有名氣)
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[求助]
C3N4沉積鎳
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最近想在C3N4上沉積鎳,參考下邊這篇文獻(xiàn)在石墨烯上沉積鎳的方法,方法如下: Preparation of GOCNTs.A series of GOCNT samples containing different amounts and lengths of CNTs were prepared. In a typical preparation,2g of sodium dodecyl sulfate (SDS, Merck) was dissolved in 40 mL of DI water. Twenty milliliters of GO dispersion of concentration 5 mg/mL was added into the above solution. The mixture was sonicated for about 20 min. Then, 1.74 g of nickel nitrate hexahydrate (Ni(NO3)2·6H2O, Alfa Aesar) dissolved in 20 mL of DI water was added dropwise under vigorous stirring. The resulting mixture was diluted with DI water to have a total volume of 120 mL and heated to 90 °C under stirring. After 16 h, the mixture was evaporated and dried in air with a Petri dish at 60 °C for 24 h to obtain Ni-loaded GO platelets. 在實(shí)驗(yàn)過(guò)程中并沒(méi)有還原劑的存在,想問(wèn)一下,在這個(gè)條件下會(huì)有Ni生成么?如果不能,需要加什么還原劑呢? 參考文獻(xiàn)題目:Pillaring Chemically Exfoliated Graphene Oxide with Carbon Nanotubes for Photocatalytic Degradation of Dyes under Visible Light Irradiation 作者:Li Li Zhang, Zhigang Xiong, and X. S. Zhao 參考文獻(xiàn)見(jiàn)附件 請(qǐng)教各路大神 前邊那個(gè)帖子的文獻(xiàn)有誤,重新上傳下,請(qǐng)各位在這個(gè)帖子回復(fù),謝謝! |

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