| 5 | 1/1 | 返回列表 |
| 查看: 595 | 回復: 2 | ||
| 當前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | ||
[求助]
birnessite晶體解析!
|
||
|
最近投了一篇稿子,這已經是第三輪大修了。詳細審稿意見如下。 (2) Structure birnessites. I appreciate a thorough literature review on the crystallography of the birnessite. However, the structure and composition of birnessite strongly depends on the synthesis conditions, especially in case of the substrate-directed growth presented in this manuscript. Therefore, it absolutely necessary to perform structure refinement in this case. The explanation provided by the Authors can be true, but if not supported by experimental refinement cannot be accepted. Without the experimental structure refinement, the Authors need to remove their strong statements related to the positions ofMn(III) and ions between the layers. This however will also impact the conclusions made by the Authors. 本人做了一個beta-MnO2上面生長birnessite的復合物。因為進行了試驗條件的調控,birnessite里面的Mn3+含量有所提高。第二輪審稿意見追問提高的Mn3+在什么位置。所以查找相關文獻加以說明!可是審稿人并不信服,要求做structure refinement!本人在這方面完全沒有接觸過,看了一些資料,完全超出能夠理解的范圍,現求助: (1)可否在beta-MnO2上面生長birnessite的復合物做structure refinement?beta-MnO2和birnessite都已確定為單晶 (2)如果可以做,我需要采集哪些數據。確認birnessite里面Mn3+和Mn4+的位置 (3)求助幫忙做structure refinement大神,金幣不多。其他方式答謝亦可! 這段時間急死了,吃不好,睡不著。希望能得到大神的幫助! |
金蟲 (小有名氣)

| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 一志愿北京理工大學本科211材料工程294求調劑 +6 | mikasa的圍巾 2026-03-28 | 6/300 |
|
|---|---|---|---|---|
|
[考研] 各位老師好,我的一志愿為北京科技大學085601材料專碩 +7 | Koxui 2026-03-28 | 7/350 |
|
|
[考研] 332求調劑 +6 | 蕉蕉123 2026-03-28 | 6/300 |
|
|
[考研] 070300化學354求調劑 +3 | 101次希望 2026-03-28 | 3/150 |
|
|
[考研] 317分 一志愿南理工材料工程 本科湖工大 求調劑 +7 | 芋泥小鈴鐺 2026-03-28 | 7/350 |
|
|
[考研] 壓國家一區(qū)線,求導師收留,有恩必謝! +7 | 迷人的哈哈 2026-03-28 | 7/350 |
|
|
[考研] 一志愿華北電力大學能動專碩,293,求調劑 +3 | 15537177284 2026-03-23 | 5/250 |
|
|
[考研] 283求調劑 +3 | A child 2026-03-28 | 3/150 |
|
|
[考研] 0703化學 +10 | 妮妮ninicgb 2026-03-27 | 10/500 |
|
|
[考研] 085405 考的11408求各位老師帶走 +3 | Qiu學ing 2026-03-28 | 3/150 |
|
|
[考研] 292求調劑 +14 | 鵝鵝鵝額額額額?/a> 2026-03-25 | 15/750 |
|
|
[考研] 311求調劑 +3 | 希望上岸阿小楊 2026-03-23 | 3/150 |
|
|
[考研] 315分求調劑 +7 | 26考研上岸版26 2026-03-26 | 7/350 |
|
|
[考研] 調劑 +3 | 李嘉圖·S·路 2026-03-27 | 3/150 |
|
|
[考研] 【雙一流院校新能源、環(huán)境材料,材料加工與模擬招收大量調劑】 +4 | Higraduate 2026-03-22 | 8/400 |
|
|
[考研] 求調劑 +8 | Auroracx 2026-03-22 | 8/400 |
|
|
[考研] 考研一志愿蘇州大學初始315(英一)求調劑 +3 | sbdksD 2026-03-24 | 4/200 |
|
|
[考研] 一志愿北化315 求調劑 +3 | akrrain 2026-03-24 | 3/150 |
|
|
[考研] 求調劑 +6 | 研研,接電話 2026-03-24 | 7/350 |
|
|
[考研] 一志愿重慶大學085700資源與環(huán)境,總分308求調劑 +7 | 墨墨漠 2026-03-23 | 8/400 |
|