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wqwang07611銀蟲(chóng) (正式寫(xiě)手)
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論文題目： Reductive Amination of 2-Amino-2-methyl-1-propanol and Ammonia to Produce 2-Methyl-1,2-propanediamine over Raney Nickel Catalyst DOI: 10.1002/slct.201701219 ChemistrySelect 2017, 2, 8818 – 8823 |
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暫沒(méi)有引用! Reductive Amination of 2-Amino-2-methyl-1-propanol and Ammonia to Produce 2-Methyl-1,2-propanediamine over Raney Nickel Catalyst 作者:Wang, WQ (Wang, Weiqiang)[ 1 ] ; Yu, QW (Yu, Qinwei)[ 1 ] ; Zhang, Q (Zhang, Qian)[ 1 ] ; Mei, SN (Mei, Suning)[ 1 ] ; Yuan, J (Yuan, Jun)[ 1 ] ; Zhao, FW (Zhao, Fengwei)[ 1 ] ; Yang, JM (Yang, Jianming)[ 1 ] ; Lu, J (Lu, Jian)[ 1 ] CHEMISTRYSELECT 卷: 2 期: 28 頁(yè): 8818-8823 DOI: 10.1002/slct.201701219 出版年: SEP 29 2017 查看期刊影響力 摘要 The selective synthesis of 2-methyl-1,2-propyldiamine (MPDA) directly from 2-amino-2-methyl-1-propanol (AMP) and ammonia via one-pot reaction is reported for the first time. The effects of catalyst species and reaction variables on the synthetic performance of MPDA were systematically studied. In contrast to other catalysts, a high MPDA selectivity of 88.3% and AMP conversion of 45.6% were obtained over Raney Ni catalyst. The components of the final reaction mixtures were particularly dependent on the initial hydrogen pressure and stirring speed. Furthermore, a possible mechanism of the reaction was proposed on the basis of experimental results, which has great implications in the development of more efficient and higher selectivity catalysts. 關(guān)鍵詞 作者關(guān)鍵詞:2-amino-2-methyl-1-propanol; 2-methyl-1,2-propyldiamine; Raney Nickel; reductive amination KeyWords Plus:SELECTIVE SYNTHESIS; PRIMARY ALCOHOLS; PRIMARY AMINES; ETHANOLAMINE; ETHYLENEDIAMINE; MORDENITE; HYDROGENATION 作者信息 通訊作者地址: Yang, JM; Lu, J (通訊作者) 顯示更多 Xian Modern Chem Res Inst, State Key Lab Fluorine & Nitrogen Chem, 168 Zhangba East Rd, Xian 710065, Shaanxi, Peoples R China. 地址: 顯示更多 [ 1 ] Xian Modern Chem Res Inst, State Key Lab Fluorine & Nitrogen Chem, 168 Zhangba East Rd, Xian 710065, Shaanxi, Peoples R China 電子郵件地址:yangjm204@163.com; lujian204@163.com 基金資助致謝 基金資助機(jī)構(gòu) 授權(quán)號(hào) Key Research and Development Projects of Shanxi Province 2017ZDXM-GY-042 2017ZDXM-GY-070 查看基金資助信息 出版商 WILEY-V C H VERLAG GMBH, POSTFACH 101161, 69451 WEINHEIM, GERMANY 類別 / 分類 研究方向:Chemistry Web of Science 類別:Chemistry, Multidisciplinary 文獻(xiàn)信息 文獻(xiàn)類型:Article 語(yǔ)種:English 入藏號(hào): WOS:000412681900016 ISSN: 2365-6549 期刊信息 Impact Factor (影響因子): Journal Citation Reports 其他信息 IDS 號(hào): FJ4CJ Web of Science 核心合集中的 "引用的參考文獻(xiàn)": 44 Web of Science 核心合集中的 "被引頻次": 0 |
2樓2017-12-18 21:31:36
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