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wqwang07611

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論文題目：
Reductive Amination of 2-Amino-2-methyl-1-propanol and
Ammonia to Produce 2-Methyl-1,2-propanediamine over
Raney Nickel Catalyst

DOI: 10.1002/slct.201701219

ChemistrySelect 2017, 2, 8818 – 8823

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wqwang07611: 金幣+5, ★★★★★最佳答案 2017-12-18 21:37:24
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暫沒有引用!
Reductive Amination of 2-Amino-2-methyl-1-propanol and Ammonia to Produce 2-Methyl-1,2-propanediamine over Raney Nickel Catalyst
作者:Wang, WQ (Wang, Weiqiang)[ 1 ] ; Yu, QW (Yu, Qinwei)[ 1 ] ; Zhang, Q (Zhang, Qian)[ 1 ] ; Mei, SN (Mei, Suning)[ 1 ] ; Yuan, J (Yuan, Jun)[ 1 ] ; Zhao, FW (Zhao, Fengwei)[ 1 ] ; Yang, JM (Yang, Jianming)[ 1 ] ; Lu, J (Lu, Jian)[ 1 ]
CHEMISTRYSELECT
卷: 2 期: 28 頁: 8818-8823
DOI: 10.1002/slct.201701219
出版年: SEP 29 2017
查看期刊影響力
摘要
The selective synthesis of 2-methyl-1,2-propyldiamine (MPDA) directly from 2-amino-2-methyl-1-propanol (AMP) and ammonia via one-pot reaction is reported for the first time. The effects of catalyst species and reaction variables on the synthetic performance of MPDA were systematically studied. In contrast to other catalysts, a high MPDA selectivity of 88.3% and AMP conversion of 45.6% were obtained over Raney Ni catalyst. The components of the final reaction mixtures were particularly dependent on the initial hydrogen pressure and stirring speed. Furthermore, a possible mechanism of the reaction was proposed on the basis of experimental results, which has great implications in the development of more efficient and higher selectivity catalysts.
關鍵詞
作者關鍵詞:2-amino-2-methyl-1-propanol; 2-methyl-1,2-propyldiamine; Raney Nickel; reductive amination
KeyWords Plus:SELECTIVE SYNTHESIS; PRIMARY ALCOHOLS; PRIMARY AMINES; ETHANOLAMINE; ETHYLENEDIAMINE; MORDENITE; HYDROGENATION
作者信息
通訊作者地址: Yang, JM; Lu, J (通訊作者)
顯示更多 Xian Modern Chem Res Inst, State Key Lab Fluorine & Nitrogen Chem, 168 Zhangba East Rd, Xian 710065, Shaanxi, Peoples R China.
地址:
顯示更多 [ 1 ] Xian Modern Chem Res Inst, State Key Lab Fluorine & Nitrogen Chem, 168 Zhangba East Rd, Xian 710065, Shaanxi, Peoples R China
電子郵件地址:yangjm204@163.com; lujian204@163.com
基金資助致謝
基金資助機構授權號
Key Research and Development Projects of Shanxi Province
2017ZDXM-GY-042
2017ZDXM-GY-070
查看基金資助信息
出版商
WILEY-V C H VERLAG GMBH, POSTFACH 101161, 69451 WEINHEIM, GERMANY
類別 / 分類
研究方向:Chemistry
Web of Science 類別:Chemistry, Multidisciplinary
文獻信息
文獻類型:Article
語種:English
入藏號: WOS:000412681900016
ISSN: 2365-6549
期刊信息
Impact Factor (影響因子): Journal Citation Reports
其他信息
IDS 號: FJ4CJ
Web of Science 核心合集中的 "引用的參考文獻": 44
Web of Science 核心合集中的 "被引頻次": 0

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張飛

2樓2017-12-18 21:31:36