| 5 | 1/1 | 返回列表 |
| 查看: 1495 | 回復(fù): 4 | ||||
| 當(dāng)前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | ||||
wwbing_2002木蟲 (正式寫手)
|
[求助]
求XPS測試高人指點
|
|||
|
近期投稿的意見返回,審稿人要求回答XPS非常細致的問題,求XPS方面的專家指點 審稿人意見: 2)The experimental details for the XPS measurements are completely inadequate and should be included in the manuscript or supporting information. The units of the pass energies are wrong (volt is a unit of potential difference, not energy). Which relative sensitivity factors were used for quantification? How were the samples mounted? How was charge neutralization performed? What was the excitation source (energy, power, monochromation)? How were the resulting spectra charge referenced? Which background type was used for integration? 審稿人問的太細太裝,但上述這些細節(jié)測試條件從哪可以獲。吭趺椿卮鸨容^好 3)The authors should include all detected elements when calculating the atomic concentrations from XPS survey spectra. They are missing calcium and sodium and silicon from the starting material, and sulfur and silicon in the product. The authors should also justify the presence of these elements considering their potential effect on the performance of the materials. 關(guān)鍵我們測的XPS只分析了C、O、N,樣品不含Ca、Si、Na,理論上XPS應(yīng)該測不出他們的信號,為什么審稿人要求考察Ca、Si、Na對材料性能的影響? |
木蟲 (正式寫手)
專家顧問 (文壇精英)
![]() |
專家經(jīng)驗: +1654 |
|
也沒有故意難為你吧,這些基本的單位,靶材,中和電荷有沒有用,怎么校正譜線的你多少應(yīng)該清楚的,不知道最好就是回去問幫你測的老師,第二個你就把全譜放上去說那幾個元素位置沒峰不含這幾個元素就可以了,當(dāng)然最理想是分別掃這幾個位置的高分辨譜,沒有信號當(dāng)然就沒有,人家只是讓你驗證一下,又不是理論上沒有就肯定測出來沒有的 發(fā)自小木蟲Android客戶端 |
木蟲 (正式寫手)
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 材料學(xué)碩318求調(diào)劑 +5 | February_Feb 2026-03-19 | 5/250 |
|
|---|---|---|---|---|
|
[考研] 288求調(diào)劑 +15 | 于海海海海 2026-03-19 | 15/750 |
|
|
[考研] 296求調(diào)劑 +3 | www_q 2026-03-18 | 6/300 |
|
|
[考研] 一志愿武漢理工材料工程專碩調(diào)劑 +5 | Doleres 2026-03-19 | 5/250 |
|
|
[考研] 本人考085602 化學(xué)工程 專碩 +17 | 不知道叫什么! 2026-03-15 | 19/950 |
|
|
[考研] 材料與化工求調(diào)劑 +7 | 為學(xué)666 2026-03-16 | 7/350 |
|
|
[考研] 一志愿南昌大學(xué),327分,材料與化工085600 +3 | Ncdx123456 2026-03-19 | 3/150 |
|
|
[考研] 材料考研調(diào)劑 +3 | xwt。 2026-03-19 | 3/150 |
|
|
[考研] 一志愿985,本科211,0817化學(xué)工程與技術(shù)319求調(diào)劑 +10 | Liwangman 2026-03-15 | 10/500 |
|
|
[考研] 332求調(diào)劑 +3 | ydfyh 2026-03-17 | 3/150 |
|
|
[教師之家] 焦慮 +9 | 水冰月月野兔 2026-03-13 | 13/650 |
|
|
[考研] 一志愿武理材料305分求調(diào)劑 +5 | 想上岸的鯉魚 2026-03-18 | 6/300 |
|
|
[考研]
|
胡辣湯放糖 2026-03-15 | 6/300 |
|
|
[考博] 26博士申請 +3 | 1042136743 2026-03-17 | 3/150 |
|
|
[考研] 277調(diào)劑 +5 | 自由煎餅果子 2026-03-16 | 6/300 |
|
|
[考研] 308求調(diào)劑 +4 | 是Lupa啊 2026-03-16 | 4/200 |
|
|
[基金申請]
今年的國基金是打分制嗎?
50+3
|
zhanghaozhu 2026-03-14 | 3/150 |
|
|
[考研] 0703 物理化學(xué)調(diào)劑 +3 | 我可以上岸的對?/a> 2026-03-13 | 5/250 |
|
|
[考研] 080500,材料學(xué)碩302分求調(diào)劑學(xué)校 +4 | 初識可樂 2026-03-14 | 5/250 |
|
|
[考研] 330求調(diào)劑 +3 | ?醬給調(diào)劑跪了 2026-03-13 | 3/150 |
|