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wwbing_2002木蟲 (正式寫手)
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[求助]
求XPS測試高人指點
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近期投稿的意見返回,審稿人要求回答XPS非常細致的問題,求XPS方面的專家指點 審稿人意見: 2)The experimental details for the XPS measurements are completely inadequate and should be included in the manuscript or supporting information. The units of the pass energies are wrong (volt is a unit of potential difference, not energy). Which relative sensitivity factors were used for quantification? How were the samples mounted? How was charge neutralization performed? What was the excitation source (energy, power, monochromation)? How were the resulting spectra charge referenced? Which background type was used for integration? 審稿人問的太細太裝,但上述這些細節(jié)測試條件從哪可以獲?怎么回答比較好 3)The authors should include all detected elements when calculating the atomic concentrations from XPS survey spectra. They are missing calcium and sodium and silicon from the starting material, and sulfur and silicon in the product. The authors should also justify the presence of these elements considering their potential effect on the performance of the materials. 關(guān)鍵我們測的XPS只分析了C、O、N,樣品不含Ca、Si、Na,理論上XPS應(yīng)該測不出他們的信號,為什么審稿人要求考察Ca、Si、Na對材料性能的影響? |
木蟲 (正式寫手)
專家顧問 (文壇精英)
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專家經(jīng)驗: +1654 |
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也沒有故意難為你吧,這些基本的單位,靶材,中和電荷有沒有用,怎么校正譜線的你多少應(yīng)該清楚的,不知道最好就是回去問幫你測的老師,第二個你就把全譜放上去說那幾個元素位置沒峰不含這幾個元素就可以了,當(dāng)然最理想是分別掃這幾個位置的高分辨譜,沒有信號當(dāng)然就沒有,人家只是讓你驗證一下,又不是理論上沒有就肯定測出來沒有的 發(fā)自小木蟲Android客戶端 |
木蟲 (正式寫手)
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