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jiaxiaopen木蟲 (小有名氣)
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[交流]
酬金求助摘要翻譯
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摘 要 以2-芳基嗎啉為先導(dǎo)化合物，利用外消旋化合物2-氨基丙醇與α-溴-芳基烷基酮反應(yīng)，合成了嗎啉環(huán)上3,5位含二甲基的新型2-芳基嗎啉類化合物3,5-二甲基-2-芳基嗎啉，經(jīng)干燥氯化氫酸化后得到其鹽酸鹽，總收率為63.7%，這在國內(nèi)外從未見有過報道,本合成路線反應(yīng)條件不苛刻，副反應(yīng)少，反應(yīng)溶劑可回收利用等特點，目標化合物結(jié)構(gòu)也已經(jīng)質(zhì)譜和核磁測試技術(shù)確證。 麻煩蟲友兄弟們幫忙翻譯一下，在此謝過，祝各位蟲友家庭幸福，工作順利。。 |
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Abstract 3,5 - dimethyl -2 - aryl morpholine,as the new kind of 2-Arylmorpholine compounds containing 3,5-dimethyl in Morpholine ring ,was synthesized by racemic compound 2-amino-propanol ,α-bromo - aryl alkyl ketones and 2 - Arylmorpholine as Lead compound.Then its hydrochloride salt was obtained by acidification by dry hydrogen chloride ,the overall yield was 63.7%.This has never been reported at home and abroad , the synthetic reaction condition is not harsh with few side effects, besides the solvent is recyclable.The structure of the target compound has been confirmed by MS and NMR . |
3樓2010-07-12 11:32:18
★ ★ ★ ★ ★
jiaxiaopen(金幣+15, 翻譯EPI+1):謝謝你的翻譯。。。祝你工作順利，萬事如意 2010-07-12 16:16:13
cfk580713(金幣+5):謝謝參與。 2010-11-30 17:23:11
jiaxiaopen(金幣+15, 翻譯EPI+1):謝謝你的翻譯。。。祝你工作順利，萬事如意 2010-07-12 16:16:13
cfk580713(金幣+5):謝謝參與。 2010-11-30 17:23:11
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Abstract 3,5 - dimethyl -2 - aryl morpholine,as the new kind of 2-Arylmorpholine compounds containing 3,5-dimethyl in Morpholine ring ,was synthesized by racemic compound 2-amino-propanol ,α-bromo - aryl alkyl ketones and 2 - Arylmorpholine as Lead compound.Then its hydrochloride salt was obtained by acidification by dry hydrogen chloride ,the overall yield was 63.7%.This has never been reported at home and abroad , the synthetic reaction condition is not harsh with few side effects, recyclable solvent characteristics such as .The structure of the target compound has been confirmed by MS and NMR . |
2樓2010-07-12 11:28:09
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