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【求助】求助:關(guān)于儀器 檢測限相關(guān)問題? 已有2人參與
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請問一個關(guān)于檢測限(LOD)和定量限(LOQ)的問題 我的一篇文章投到analytical chimica acta之后,編輯一直問一個關(guān)于LOD和 LOQ的問題。我定義了檢測限為3倍信噪比,定量限為10倍信噪比。我做的時候是標準樣品倍比稀釋,濃度分別為40, 20, 10, 5, 2.5μg/kg,然后用HPLC檢測,得到的LOD5μg/kg,為LOQ10μg/kg。但是編輯認為我既然定義了檢測限為3被信噪比,定量限為10 被倍信噪比,那么定量限應(yīng)該為檢測限的3.3倍,可是我的濃度本來就是倍比稀釋的啊,信噪比大于10的最低濃度為10μg/kg,信噪比大于3的最低濃度為5μg/kg。 我不知道怎么解釋他們才能聽懂,還是我應(yīng)該改變檢測限和定量限的定義呢?著急,謝謝好心人! 如下是編輯的comments In your response to my comments you have written "We defined LOD as the lowest drug concentration in the samples can be measured with a signal to the background signal (S/N) ratio of 3/1(S/N), and LOD as the lowest drug concentration in food samples can be measured with a signal to the background signal (S/N) ratio of 10/1(S/N). After the detection, we found that the LOD was 5 |
金蟲 (小有名氣)


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