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zhigang985銀蟲 (小有名氣)
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[求助]
求助高手翻譯一段話，謝謝！
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（1）x微米球的TEM(a, b)、HRTEM(c, d)圖及x=0.1 mol/L時(shí)，120 ℃反應(yīng)24 h制得產(chǎn)物x的TEM(e)、HRETEM(f)圖 （2）根據(jù)實(shí)驗(yàn)的結(jié)果，我們提出了x空心微米球可能形成的形成機(jī)理：首先，乙二胺與x溶液混合形成配合物[x(en)2]2+，然后配合物離解生成的en與透過油膜的CS2發(fā)生反應(yīng)(2)，(2)式中形成的中間體再發(fā)生縮聚反應(yīng)(3)生成H2S，H2S作為反應(yīng)的S2-源與x發(fā)生反應(yīng)(4)生成xS納米晶�？赡艿姆磻�(yīng)如下 |
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【答案】應(yīng)助回帖
★
zhigang985(金幣+10, 翻譯EPI+1): 2011-05-02 22:20:48
sltmac(金幣+1): 謝謝交流，歡迎常來~~ 2011-05-03 12:36:19
zhigang985(金幣+10, 翻譯EPI+1): 2011-05-02 22:20:48
sltmac(金幣+1): 謝謝交流，歡迎常來~~ 2011-05-03 12:36:19
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翻譯不精，僅供參考。 The TEM (a, b) of X microns ball, HRTEM (c, d) chart and x = 0.1 mol/L, the TEM (e), HRETEM (f) chart of the production X were achieved under the conditions of 120 ℃, 24 h. According to the experimental results, we proposed the mechanism that x hollow microns ball might be formed: first, ethylenediamine and X solution were mixed to form complexes [x (en) 2] 2 +, then en generated by complexes dissociation reacted with CS2 penetrated through oil film, as reaction (2), polycondensation reaction (3) by intermediate generated in reaction (2) produced H2S,which reacted with X as the S2- source to generate XS nanocrystalline, as reaction (4). The possible reactions were as follows: |
2樓2011-05-02 21:18:36
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