 |
 |
 |
 |
 |
 |
||
 |
 |
 |
 |
 |
| 5 | 1/1 | 返回列表 |
| 查看: 1653 | 回復(fù): 8 | ||
| 當(dāng)前只顯示滿足指定條件的回帖，點(diǎn)擊這里查看本話題的所有回帖 | ||
[求助]
acta e 審稿意見回來，請教��！如何修改和回復(fù)@~~~~~~~~~~~~~
|
||
|
Your paper can be accepted after taking into account the following comments: 1. Abstract: plural in first sentence ..... oxazole goups. second sentence: The complex is six-coordinate ... geometry. or better: The six-coordinate complex displays a distorted octahedral geometry. 2. last sentence: the Cg...Cg distance and symmetry operations must be given. However, the two oxazole units have two five-membered and six six-membered rings. this implies a lot of work defining the centres of gravity (Cg's) for the rings and calculating the distances between Cg's and average perpendicular distances between the ring systems. Moreover, your Fig. 2 does not show the inversion related \p--\p interaction clearly, and the symmetry operators for molecule A and molecule B should also be provided in the caption of Figure 2. You need a programme like PLATON which can help analize this problem by using the "cal all" option. It will also be seen that the complexes are held together by a combination of different \p--\p interactions and a C---H...\p contact when PLATON is applied. (see point 9) The best was to delete the sentence in Abstract ... exhibits obvious intermolecular \p--\p interactions and also delete Fig. 2. Otherwise, details must be calculated, which needs time ... IMPORTANT: all numerical measured values need standard uncertainties (s.u.), which will be described for the Comment section. 3. Computing details: the SHELXS97 and SHELXL97 reference must refer to a new reference: Sheldrick, G. M. (2008). Acta Cryst. A64, 112--122. please use this reference instead of the Sheldrick G. M. (2001). reference please download and read this article which will show you that the Bruker AXS SHELXTL programme should be cited with the new Sheldrick (2008) reference. 3. in the computing details block it should be corrected like: _computing_structure_solution 'SHELXS97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL97 (Sheldrick, 2008)' _computing_molecular_graphics 'SHELXTL (Sheldrick, 2008)' _computing_publication_material 'SHELXL97 ' 4. References: Abbady M. A. (1979). .... there is only one author, delete the Assiut ... Assiut E. part there 5. Comment, please short: ... has been reported (Lamansky et l., 2001), among ... please write the trivial names for the ligands (bo) and (bon) in the long introductory sentence, as they appear only once in the text. 6. Comment: please think of having two oxazol ligands, so the average deviation of Ir1 C18 C23 C24 N2 and the dihedral angles as for molecule 1 (average is 0.0628 and 0.0719 (typo mol. 1, please check, and mol. 2) the s.u.'s for dihedral angles in parentheses: 6.5(2)\% (6.9(1)\% for mol.2), 9.2(1)\% (11.4(1)\% for mol. 2). please check with MPLA in SHELXL97. 7. Comment: please shorten the text by using just one sentence which refers to Table 1. two values each averaged not necessary. (Relevant coordination distances shown in Table 1.) 8. Table 1: please show only the six Ir---C/N/O bond distances and omit other distances and angles by replacement of yes with ? in the cif tables. The values are kept with the Supplementary materials. 9. Fig. 2: delete in Text in the Comment or you may download the programme PLATON and chose two inversion related \p--\p interactions with details as proposed in point 2, and the weak C26---H26...Cg9 contact. Cg9 is the centroid of ring C18 - C23, symmetry operation -x, y, 3/2 - z for the \p--\p interactions please chose two examples Cg3...Cg3i and Cg3...Cg6i (there are many others) the rings are parallel and inversion related. symmetry code i (7_556) is 1/2 - x, 1/2 - y, 1 - z -------------------------------------------------------- PLATON download is recommended via http://www.cryst.chem.uu.nl/platon/p1000000.html help-files are also available there for Windows systems download WinPLATON via http://www.chem.gla.ac.uk/~louis/software/platon/ A short PLATON tutorial is offered by Lachlan Cranswick at http://www.ccp14.ac.uk/tutorial/platon/index.html --------------------------------------------------------------- 10. Experimental, reference: .... to the literature (Abbady, 1979). Please send me an email indicating how you have responded to each of the comments. You should upload a new CIF at the web address: http://submission.iucr.org/submi ... Xaz7dXI43jLy/si2371 Please acknowledge receipt of this message as soon as you see it, so that I know it has arrived safely. Best wishes |
回復(fù)此樓» 猜你喜歡
數(shù)一英一271專碩（085401）求調(diào)劑，可跨
已經(jīng)有8人回復(fù)
-
295求調(diào)劑
已經(jīng)有4人回復(fù)
-
0856求調(diào)劑
已經(jīng)有5人回復(fù)
-
材料學(xué)碩333求調(diào)劑
已經(jīng)有10人回復(fù)
-
299求調(diào)劑
已經(jīng)有6人回復(fù)
-
一志愿鄭州大學(xué)，080500學(xué)碩，總分317分求調(diào)劑
已經(jīng)有6人回復(fù)
-
289求調(diào)劑
已經(jīng)有12人回復(fù)
-
070305高分子化學(xué)與物理 304分求調(diào)劑
已經(jīng)有6人回復(fù)
-
0703化學(xué)調(diào)劑，求導(dǎo)師收
已經(jīng)有10人回復(fù)
-
各位老師好，我的一志愿為北京科技大學(xué)085601材料專碩
已經(jīng)有5人回復(fù)
» 本主題相關(guān)價值貼推薦，對您同樣有幫助:
- 急求ACTA E 審稿意見回復(fù)
已經(jīng)有3人回復(fù)
- 請教Appliced optics 修改意見中為什么只看到一個審稿人的意見？
已經(jīng)有9人回復(fù)
- 投了ACTA，返回大修，審稿人問到數(shù)據(jù)重現(xiàn)性的問題，如何回答？
已經(jīng)有7人回復(fù)
- acta E 審稿意見回復(fù)（語法方面的)，萬急！~~~~~ 請高手看下！
已經(jīng)有7人回復(fù)
- 【請教】請教acta e審稿意見
已經(jīng)有4人回復(fù)
- 審稿意見回來了，有些地方看不明白，請教大家
已經(jīng)有3人回復(fù)
- 審稿意見回復(fù)請教
已經(jīng)有4人回復(fù)
- 【請教】投稿acta e 后被拒，修改后再投稿...
已經(jīng)有11人回復(fù)
- 審稿意見回來。請教投過國際氫能源的蟲友啊
已經(jīng)有17人回復(fù)
7樓2011-08-18 14:36:27
2樓2011-08-18 12:09:07
yguang
木蟲 (職業(yè)作家)
- 應(yīng)助: 24 (小學(xué)生)
- 金幣: 12850.8
- 紅花: 14
- 帖子: 4683
- 在線: 618.4小時
- 蟲號: 696608
- 注冊: 2009-02-05
- 專業(yè): 微生物遺傳育種學(xué)
3樓2011-08-18 12:16:43
4樓2011-08-18 12:22:01
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 一志愿211 初試270分 求調(diào)劑 +7 | 谷雨上岸 2026-03-23 | 8/400 |
|
|---|---|---|---|---|
|
|
[考研] 求調(diào)劑 +7 | 爭取九點(diǎn)睡 2026-03-28 | 8/400 |
|
|
|
[考研] 化學(xué)0703 調(diào)劑 306分 一志愿211 +4 | 26要上岸 2026-03-28 | 4/200 |
|
|
|
[考研] 復(fù)試調(diào)劑 +3 | raojunqi0129 2026-03-28 | 3/150 |
|
|
[考研] 材料與化工（0856）304求B區(qū)調(diào)劑 +8 | 邱gl 2026-03-27 | 8/400 |
|
|
|
[考研] 085701環(huán)境工程，267求調(diào)劑 +16 | minht 2026-03-26 | 16/800 |
|
|
|
[考研] 一志愿哈爾濱工業(yè)大學(xué)材料與化工方向336分 +8 | 辰沐5211314 2026-03-26 | 8/400 |
|
|
|
[考研] 藥學(xué)105500求調(diào)劑 +3 | Ssun。。 2026-03-28 | 3/150 |
|
|
|
[考研] 材料求調(diào)劑 一志愿哈工大總分298分，前三科223分 +5 | dongfang59 2026-03-27 | 5/250 |
|
|
|
[考研] 材料與化工085600，總分304，本科有兩篇sci參與，求調(diào)劑 +10 | 幸運(yùn)的醬醬 2026-03-22 | 12/600 |
|
|
|
[考研] 085600，材料與化工321分，求調(diào)劑 +9 | 大饞小子 2026-03-27 | 9/450 |
|
|
|
[考研] 一志愿吉大071010，316分求調(diào)劑 +3 | xgbiknn 2026-03-27 | 3/150 |
|
|
|
[考研] 284求調(diào)劑 +11 | junqihahaha 2026-03-26 | 12/600 |
|
|
|
[考研] 317求調(diào)劑 +7 | 蛋黃咸肉粽 2026-03-26 | 7/350 |
|
|
|
[考研] 341求調(diào)劑 +7 | 青檸檬1 2026-03-26 | 7/350 |
|
|
|
[考研] 352求調(diào)劑 +4 | 大米飯！ 2026-03-22 | 4/200 |
|
|
|
[考研] 085600 材料與化工 329分求調(diào)劑 +9 | Mr. Z 2026-03-25 | 9/450 |
|
|
|
[考研] 材料與化工328分調(diào)劑 +6 | 。，。，。，。i 2026-03-23 | 6/300 |
|
|
|
[考研] 上海電力大學(xué)材料防護(hù)與新材料重點(diǎn)實(shí)驗室招收調(diào)劑研究生（材料、化學(xué)、電化學(xué)，環(huán)境） +4 | 我愛學(xué)電池 2026-03-23 | 4/200 |
|
|
|
[考研] 080500求調(diào)劑 +3 | zzzzfan 2026-03-24 | 3/150 |
|