| 5 | 1/1 | 返回列表 |
| 查看: 1971 | 回復(fù): 3 | |||
| 當(dāng)前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | |||
qinshihuang木蟲 (正式寫手)
|
[求助]
跪求大神幫忙解決A類錯誤
|
||
|
請高手解了好久,感覺已經(jīng)沒什么問題了,仍然存在一個A類錯誤,不知道還能不能解決啊,是不是不解決就一定不能發(fā)文章了,請大神幫忙啊 Alert level A PLAT601_ALERT_2_A Structure Contains Solvent Accessible VOIDS of . 417 A**3 PLAT601 -------------------------------------------------------------------------------- PLAT601 Type_2 Test for (Unreported) solvent accessible voids -------------------------------------------------------------------------------- Crystal structures in general do not contain large solvent accessible voids in the lattice. Most structures lose their long-range ordering when solvent molecules leave the crystal. Only when the remaining network is strongly bonded (e.g. zeolites and some hydrogen bonded networks) the crystal structure may survive. Residual voids in a structure may indicate the omission of (disordered) density from the model. Disordered density may go undetected when smeared since peak search programs are not designed to locate maxima on density ridges. The presence or absence of residual density in the void may be verified on a printed/plotted difference Fourier map or with PLATON/SQUEEZE. Voids of 40 Ang**3 may accommodate H2O. Small molecules such as Tetrahydrofuran have typical volumes in the 100 to 200 Ang**3 range. This test reports the volume of the largest solvent accessible void in the structure. A paper reporting a crystal structure with a significant solvent accessible void should at the least discuss the issue. 這該如何解決啊,這個晶體是用高溫固相合成的,怎么會存在什么溶劑分子啊,更不會有H鍵啊,難道就不能存在一個很大的孔洞嗎,真的不知道該怎么解決了,還請大神幫忙,這個晶體是頂著各種壓力才做出來的,不能半途而廢啊 |
| 高檔次文章中有A級錯誤的多得是。特別是MOF類的有你這個A很常見。關(guān)鍵是你在文章中要正確的說明此孔洞。 |
木蟲 (正式寫手)
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 267求調(diào)劑 +9 | uiybh 2026-03-31 | 9/450 |
|
|---|---|---|---|---|
|
[論文投稿]
chinese chemical letters英文版投稿求助
130+4
|
Yishengeryi 2026-03-30 | 4/200 |
|
|
[考研] 085600 一志愿9 總分351 求調(diào)劑學(xué)校 +7 | czhcz 2026-03-31 | 7/350 |
|
|
[考研] 346求調(diào)劑 一志愿070303有機(jī)化學(xué) +11 | 蘿卜燉青菜 2026-03-28 | 12/600 |
|
|
[考研] 08開頭看過來!! +3 | wwwwffffff 2026-03-31 | 5/250 |
|
|
[考研] 化學(xué)工程085602 305分求調(diào)劑 +28 | RichLi_ 2026-03-25 | 36/1800 |
|
|
[考研] 一志愿西電085401數(shù)一英一299求調(diào)劑 六級521 +4 | 愛吃大鴨梨 2026-03-31 | 4/200 |
|
|
[考研] 0856調(diào)劑 +6 | 曲聽筠 2026-03-30 | 6/300 |
|
|
[考研] 本科211總分289,08工學(xué)真心求調(diào)劑 +3 | utopiaE 2026-03-30 | 3/150 |
|
|
[考研] 求調(diào)劑,一志愿 南京航空航天大學(xué) ,080500材料科學(xué)與工程學(xué)碩,總分289分 +9 | @taotao 2026-03-29 | 9/450 |
|
|
[考研] 生物學(xué)學(xué)碩,一志愿湖南大學(xué),初試成績338 +7 | YYYYYNNNNN 2026-03-26 | 9/450 |
|
|
[考研] 332求調(diào)劑 +14 | 032500 2026-03-25 | 14/700 |
|
|
[考研] 一志愿南開大學(xué)0710生物學(xué)359求調(diào)劑 +5 | 兔兔兔111223314 2026-03-29 | 7/350 |
|
|
[考研] 293求調(diào)劑 +3 | 末未mm 2026-03-30 | 5/250 |
|
|
[考研] 一志愿雙一流機(jī)械285分求調(diào)劑 +4 | 幸運的三木 2026-03-29 | 5/250 |
|
|
[考研] 308求調(diào)劑 +7 | 墨墨漠 2026-03-27 | 7/350 |
|
|
[考研] 331環(huán)境科學(xué)與工程求調(diào)劑 +3 | 熠然好運氣 2026-03-27 | 3/150 |
|
|
[考研] 復(fù)試調(diào)劑,一志愿南農(nóng)083200食品科學(xué)與工程 +5 | XQTJZ 2026-03-26 | 5/250 |
|
|
[考研] 材料求調(diào)劑 +5 | .m.. 2026-03-25 | 5/250 |
|
|
[考研] 292求調(diào)劑 +4 | 求求了收下我吧?/a> 2026-03-26 | 4/200 |
|