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[求助]
吸收方法校正是怎么回事?氫原子的精修方法到底應該選那個?
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The real refinement of the hydrogen atoms should be described. This is not the case. The refinement of the hydroxyl H-atom H1 should be described. Was the atom localized by difference electron density determination. Why and which riding model was used? HFIX 83, HFIX 87 or HFIX 147 and why? Why was this hydrogen atom not refined free e.g. with restraints to the O-H distance? Check also the SHELXL manual for that. In the cif-file a min. and max. transmission value was given, but no method of absorption correction. Was there an absorption correction applied? ?and which type? Using the APEX2 Software Suite usually always an absorption correction is applied (SADABS). 這是編輯 發(fā)的信,說我的不細致。吐血! ![]() ![]() ![]() ![]() ![]() ![]() ![]() |


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