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sirius8528木蟲 (正式寫手)
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[求助]
晶體解析的問題求指教
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| 手頭上有兩個已解好的晶體,check后發(fā)現(xiàn)有一個馬馬虎虎,有一個錯誤挺多,老板讓我自己修一下,我完全不懂這方面的知識。有沒有好心人指點(diǎn)一下,有什么易上手的方法,感激不盡! |
木蟲 (正式寫手)
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Alert level A SHFSU01_ALERT_2_A The absolute value of parameter shift to su ratio > 0.20 Absolute value of the parameter shift to su ratio given 1.238 Additional refinement cycles may be required. PLAT043_ALERT_1_A Check Reported Molecular Weight ................ 142.02 PLAT051_ALERT_1_A Mu(calc) and Mu(CIF) Ratio Differs from 1.0 by . 58.77 Perc. PLAT053_ALERT_1_A Minimum Crystal Dimension Missing (or Error) ... ? PLAT054_ALERT_1_A Medium Crystal Dimension Missing (or Error) ... ? PLAT055_ALERT_1_A Maximum Crystal Dimension Missing (or Error) ... ? PLAT080_ALERT_2_A Maximum Shift/Error ............................ 1.24 PLAT122_ALERT_1_A No _symmetry_space_group_name_H-M Given ........ ? PLAT306_ALERT_2_A Isolated Oxygen Atom (H-atoms Missing ?) ....... O3 |
木蟲 (著名寫手)

木蟲 (正式寫手)
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Alert level B PLAT052_ALERT_1_B Info on Absorption Correction Method Missing ... ? Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............ 0.40 Ratio PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... ? PLAT166_ALERT_4_C S.U's Given on Coordinates for calc-flagged .... H7 PLAT324_ALERT_2_C Check for Possibly Missing H on Coordinating.... N2 PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0093 Ang |
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