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[求助]
求助這些錯(cuò)誤是什么
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有沒有高手辦我看看這些都是什么錯(cuò)誤? Alert level A EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 EXPT010_ALERT_1_A _exptl_crystal_colour (_pd_char_colour for powder) is missing Crystal colour. The following tests will not be performed. CRYSC_01 DIFF005_ALERT_1_A _diffrn_measurement_method is missing Mode of intensity measurement and scan. DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. --------------------------------------------------------------------------------Alert level C PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given ..... ? Do ! PLAT220_ALERT_2_C Large Non-Solvent O Ueq(max)/Ueq(min) ... 3.7 Ratio PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N4 --------------------------------------------------------------------------------Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 3 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 26 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 15 PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 10.05 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) La1 -- O12 .. 5.9 su PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 25 % PLAT303_ALERT_2_G Full Occupancy H-Atom H5B with # Connections 2.00 PLAT774_ALERT_1_G Suspect X-Y Bond in CIF: LA1 -- NI2 .. 3.52 Ang. And 2 other PLAT774 Alerts More ...PLAT774_ALERT_1_G Suspect X-Y Bond in CIF: LA1 -- NI2 .. 3.52 Ang. PLAT774_ALERT_1_G Suspect X-Y Bond in CIF: LA1 -- NI1 .. 3.56 Ang. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 5 H2 O PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 6 K PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 494 |

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