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875705809金蟲 (小有名氣)
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[求助]
此審稿意見該怎么回
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本人投了Organic & Biomolecular Chemistry, 一個(gè)月前修改意見,說要我補(bǔ)一個(gè)核磁數(shù)據(jù),但是那個(gè)產(chǎn)物不穩(wěn)定,我就做了一個(gè)核磁滴定,因?yàn)槠渌愃频奈恼露际沁@么弄的,結(jié)果昨天審稿意見又回來了他是這么說的: The authors claim about the instability of the so-called “compound 3” and their inability to isolate it. Which one of the two products of the reaction between 2 with Na2SO3 is unstable?. Maybe both of them?. If they/it are so unstable, how the authors have achieved the NMR and ESI studies?. How the authors checked its/their instability?. Have the authors attempted to separate them by HPLC?. I think this crucial part of the manuscript has too many unknowns to be answered. 我該怎么回復(fù)他呢?直接查相關(guān)的文獻(xiàn),說明它不穩(wěn)定,還是要怎么弄呢?請高手指點(diǎn)! 謝謝各位的幫忙! |

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