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andyzhu木蟲 (正式寫手)
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[交流]
被這樣的審稿意見拒搞了。
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雖然我知道有自己疏忽的問題,但是相對(duì)于第二個(gè)審稿人(提出更多實(shí)質(zhì)意義的的建議)讓我大修,我還是有點(diǎn)郁悶。哎,運(yùn)氣不好,還是我沒意識(shí)到這些問題有多嚴(yán)重,請(qǐng)高手指點(diǎn)迷津。如下。 1. The .cif files do not contain the shelx instructions or the reflection intensities. The .fcf file has also not been provided by the authors. As such, the refinement cannot be independently verified by the reviewer. 沒上傳fcf,是最大的罪過。 2. The text mentions the MOF space group is Pcca, however it is listed as Pccn in the .cif files. 我的錯(cuò),眼神不好,寫錯(cuò)。 3. Page 10, line 208: “Moreover, the presence of trace (CH2)2NH2+ ions used as the counter cations…” Trace ions?!? Isn’t the dimethyl ammonium the counter ion for the structure? I would expect it to be present in stoichiometric proportions, not trace amounts…自己表達(dá)不清。 4. The authors claim that the (CH2)2NH2+ ion is the charge balancing cation in the MOF structures, however, the authors present no evidence to support this claim. Given that the authors claim that the cation influences the physical properties of the material (Page 10 line 208), the chemical identity of the cation should be established unambiguously.給我個(gè)機(jī)會(huì),我可證明,的確 (CH2)2NH2+真實(shí)存在。。 5. Several notable entries in the crystal data table (S1) are absent: number of parameters, number of restraints, cell volume, 2-theta range, Rint, hkl limits.我可以補(bǔ)的,但是我的表格就是抄的這個(gè)雜志之前table。。 6. None of the datablock names in the .cif files or cifchecks matches the names in the manuscript. This unnecessarily complicates reviewer evaluations.難道我的cif命名為我的CCDC號(hào)也是一種錯(cuò)誤?不解。。 7. The Eu structure contains 12 restraints. No details are given. 之前投稿沒注意這個(gè)要。以后大家要注意了,特別是晶體學(xué)雜志 8. The H2DDQ structure: H1 does not appear to be in a correctly refined position. Likewise, the protons on the water molecule have not been refined. It seems that they should be added such that they form hydrogen bonds with N2 and O2. 9. Both the Eu and Er structures contain very large residual electron density peaks. The location of the peaks should be mentioned and explained.稀土金屬容易出現(xiàn)鬼峰,我就少說了一句。 10. While MOF datasets are often of poor quality and low resolution/completeness, this should not be the case for well-packed small molecules. Though the completeness is reasonable at 0.977, why is this not closer to 1.0? Was the data collected properly? Was there a problem with the data processing? 完整度0.977在我們學(xué)校測(cè)試可以了,曝光時(shí)間3S, 三斜掃一般700張 11. For all structures, the formulas should be updated to reflect the refined data. Atoms which are not present (for example, Cl and P in the H2DDQ structure) should be removed. 因?yàn)轶w系有這個(gè)元素,解的時(shí)候定了P Cl了,但是這不至于拒搞吧。 |
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鐵桿木蟲 (文壇精英)
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樓主稿子里估計(jì)跟該雜志要求相悖的東西太多了(尤其是技術(shù)格式和文件上傳要求等等),被審稿人這么一羅列出來,編輯一看肯定拒稿啊!其實(shí)這種情況換到任何雜志(國(guó)內(nèi)的不算、收費(fèi)水貨不算)都要被拒稿的,因?yàn)椴环险撐纳蟼饕罅耍绻夹g(shù)審查在前的話,都不用送審就直接拒了。 這不是運(yùn)氣不好,這是犯錯(cuò)太多!打鐵還需自身硬。 |

新蟲 (知名作家)
榮譽(yù)版主 (文壇精英)

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至尊木蟲 (職業(yè)作家)

木蟲 (職業(yè)作家)
| 哥們。主要是你的CIF文件與論文中多處存在不一致的地方,這種稿件,一方面體現(xiàn)投稿者自身業(yè)務(wù)不熟,第二,體現(xiàn)投稿人態(tài)度不認(rèn)真,這樣的稿件,我也會(huì)直接拒掉的。 |

| 祝福。。。。。。。。。。。 |
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