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[求助]
TPR問題的討論 已有3人參與
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我的審稿意見回復(fù)說TPR試驗(yàn)樣品數(shù)據(jù)測(cè)得少,并不能說明峰位置相相對(duì)應(yīng)的物種,可是別的文獻(xiàn)都是這樣確定的啊,求哪位高手指點(diǎn)一下該怎么回復(fù)呢?萬分感謝,審稿意見原文:The interpretation of the TPR data is sometimes risky. E.g. shifting of rather broad peaks at low intensity levels is usually not conclusive without making an extensive series of experiments of samples with gradually increasing composition. The current number of samples is too small and their composition too broad to arrive at such conclusions. The conclusions about the presence of spinel type Ni or Co containing species needs to be revisited. It is well known that during TPR, due to its nature of being a dynamic technique, such species are easily formed in-situ. Similar comments can be made about the apparent shifting of the high temperature (average) peaks. Usually this is due to the varying intensity of individual (sub) peaks. Without deconvolution of such average peaks it can be risky to make conclusions about their nature or the nature of the species involved. |

金蟲 (正式寫手)
木蟲 (正式寫手)
鐵桿木蟲 (正式寫手)

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