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沒(méi)做過(guò)類(lèi)似的結(jié)果分析,翻譯出來(lái)總感覺(jué)不太通順,求翻譯。。!
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| Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. The test was performed using a bending mode with an amplitude of 5 mm. Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. |

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Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. 在氮?dú)猸h(huán)境中,以每分鐘上升10攝氏度的加熱效率,運(yùn)用鉑金埃爾默公司研制的 DSC7號(hào)儀器,進(jìn)行差示掃描量熱。同時(shí),在氮氧環(huán)境中,以每分鐘上升20攝氏度的加熱效率,運(yùn)用鉑金埃爾默公司的Pyris1號(hào)儀器,進(jìn)行熱重分析。 Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. 運(yùn)用鉑金埃爾默公司研制Pyris Diamond號(hào)分析儀對(duì)大小為2.0cm*1.0cm*0.2cm的樣本,進(jìn)行動(dòng)態(tài)力學(xué)分析。 The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. 溫度掃描模型被調(diào)試為每分鐘升溫5攝氏度,1Hz的頻率,測(cè)量?jī)?chǔ)能模量E 和介質(zhì)損耗因數(shù)作為樣品參數(shù)。 The test was performed using a bending mode with an amplitude of 5 mm. 該項(xiàng)測(cè)試是在振幅為5mm的彎曲模態(tài)上進(jìn)行的。 Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. 以每分鐘上升5攝氏度的加熱效率,運(yùn)用鉑金埃爾默公司研制的 Pyris Diamond儀器,進(jìn)行熱機(jī)分析。 NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. 運(yùn)用600HZ高磁場(chǎng)核磁共振儀,以氘代二甲亞砜作試劑,進(jìn)行核磁共振測(cè)量。 通過(guò)將氘代二甲亞砜的化學(xué)位移設(shè)定在2.49ppm,從而校準(zhǔn)化學(xué)位移。 The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. 運(yùn)用Nicolet Avatar 320傅里葉紅外光譜儀,記錄本實(shí)驗(yàn)的紅外光譜。 |
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