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| Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. The test was performed using a bending mode with an amplitude of 5 mm. Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. |
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朱巖0308: 金幣+28, 翻譯EPI+1, ★★★★★最佳答案, 多謝 2015-03-05 14:58:15
朱巖0308: 金幣+28, 翻譯EPI+1, ★★★★★最佳答案, 多謝 2015-03-05 14:58:15
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Differential scanning calorimetry (DSC) was performed using a Perkine-Elmer DSC 7 in a nitrogen atmosphere at a heating rate of 10 C/min. Thermal gravimetric analysis (TGA) was performed with a PerkineElmer Pyris1 at a heating rate of 20 C/min in a nitrogen or air atmosphere. 在氮氣環(huán)境中，以每分鐘上升10攝氏度的加熱效率，運用鉑金埃爾默公司研制的 DSC7號儀器，進行差示掃描量熱。同時，在氮氧環(huán)境中，以每分鐘上升20攝氏度的加熱效率，運用鉑金埃爾默公司的Pyris1號儀器，進行熱重分析。 Dynamic mechanical analysis (DMA) was performed with a PerkineElmer Pyris Diamond DMA with a sample size of 2.0 1.0 0.2 cm. 運用鉑金埃爾默公司研制Pyris Diamond號分析儀對大小為2.0cm*1.0cm*0.2cm的樣本，進行動態(tài)力學分析。 The storage modulus E' and tan d were determined as the sample was subjected to the temperature scan mode at a programmed heating rate of 5 C/min at a frequency of 1 Hz. 溫度掃描模型被調試為每分鐘升溫5攝氏度，1Hz的頻率，測量儲能模量E 和介質損耗因數作為樣品參數。 The test was performed using a bending mode with an amplitude of 5 mm. 該項測試是在振幅為5mm的彎曲模態(tài)上進行的。 Thermal mechanical analysis (TMA) was performed with a PerkineElmer Pyris Diamond TMA at a heating rate of 5 C/min. 以每分鐘上升5攝氏度的加熱效率，運用鉑金埃爾默公司研制的 Pyris Diamond儀器，進行熱機分析。 NMR measurements were performed using a Varian Inova 600 NMR in DMSO-d6, and the chemical shift was calibrated by setting the chemical shift of DMSO-d6 as 2.49 ppm. 運用600HZ高磁場核磁共振儀，以氘代二甲亞砜作試劑，進行核磁共振測量。 通過將氘代二甲亞砜的化學位移設定在2.49ppm，從而校準化學位移。 The infrared spectra were recorded using a Nicolet Avatar 320 FTIR spectrophotometer. 運用Nicolet Avatar 320傅里葉紅外光譜儀，記錄本實驗的紅外光譜。 |
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