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小木蟲論壇-學(xué)術(shù)科研互動平臺 » 材料區(qū) » 晶體 » 粉末晶體 » 跪求XRD中的RIR值
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老全lq金蟲 (正式寫手)
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[求助]
跪求XRD中的RIR值 已有1人參與
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| 我現(xiàn)在急需PDF#48-1278（TiO2）和PDF#50-0791（Ti9O17)在PDF卡片中的RIR值，在做半定量分析。麻煩數(shù)據(jù)庫里有此數(shù)據(jù)的分享一下，非常感謝。 |
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PDF#85-1061: QM=Calculated(C); d=Calculated; I=Calculated Titanium Oxide Ti9 O17 Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=6.035-63.308 I/Ic(RIR)=1.01 Ref: Calculated from ICSD using POWD-12++ (1997) Triclinic - (Unknown), I-1 (2) Z=4 mp= CELL: 5.524 x 7.142 x 50.03 <66.41 x 57.2 x 108.53> P.S=aP52 (?) Density(c)=4.265 Density(m)=5.02A Mwt=703.09 Vol=547.36 F(30)=311.3(.0019,52/0) Ref: le Page, Y., Strobel, P. J. Solid State Chem., v44 p273 (1982) Strong Lines: 3.07/X 3.17/8 3.34/7 3.65/4 1.68/4 2.50/4 1.70/4 2.49/4 2.55/3 1.64/3 FIZ=035124: ICSD SG: I1- IT is: 2 SG short form: I-1 ITF See PDF 00-050-0791. Structural chemistry of the Magneli phases Tin O(2n-1), 4<=n<=9 i25 c a (I1-) N9O17 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 6.035 14.6327 3.4 ( 0 0 2) 3.018 0.0342 0.4294 12.087 7.3163 1.5 ( 0 0 4) 6.043 0.0683 0.8588 13.165 6.7194 0.1 ( 0 1 5) 6.583 0.0744 0.9351 13.791 6.4157 0.1 ( 0 1 3) 6.896 0.0779 0.9794 15.164 5.8379 0.1 ( 0 1 7) 7.582 0.0856 1.0763 16.933 5.2319 1.9 ( 1 0 7) 8.466 0.0956 1.2009 17.720 5.0011 4.0 ( 1 0 5) 8.860 0.1000 1.2564 18.173 4.8776 1.5 ( 0 0 6) 9.086 0.1025 1.2882 18.258 4.8551 1.6 ( 1 0 9) 9.129 0.1030 1.2942 18.993 4.6688 0.1 ( 0 1 9) 9.496 0.1071 1.3458 19.102 4.6422 0.1 (-1 1 0) 9.551 0.1077 1.3535 20.384 4.3531 9.4 ( 1 0 3) 10.192 0.1149 1.4434 21.121 4.2029 0.1 ( 0-1 1) 10.561 0.1190 1.4950 21.121 4.2029 0.1 ( 1-1 6) 10.561 0.1190 1.4950 21.317 4.1646 0.9 ( 1 0 11) 10.659 0.1201 1.5087 22.064 4.0253 0.1 (-1 1 2) 11.032 0.1242 1.5609 24.340 3.6538 44.4 ( 0 0 8) 12.170 0.1368 1.7196 24.340 3.6538 44.4 ( 1 0 1) 12.170 0.1368 1.7196 24.936 3.5679 0.3 ( 1-1 8) 12.468 0.1401 1.7610 25.522 3.4873 1.1 ( 1 0 13) 12.761 0.1434 1.8017 26.513 3.3591 18.6 (-1 2 3) 13.256 0.1488 1.8705 26.513 3.3591 18.6 ( 0 2 10) 13.256 0.1488 1.8705 26.641 3.3432 66.8 (-1 2 1) 13.321 0.1496 1.8794 27.779 3.2088 9.0 (-1 2 5) 13.890 0.1558 1.9581 27.779 3.2088 9.0 ( 0 2 6) 13.890 0.1558 1.9581 28.147 3.1678 79.3 ( 1-2 1) 14.073 0.1578 1.9835 29.100 3.0661 100.0 (-1 0 1) 14.550 0.1631 2.0493 30.279 2.9494 3.8 (-1 2 7) 15.139 0.1695 2.1303 30.350 2.9426 5.1 ( 0 2 4) 15.175 0.1699 2.1352 30.438 2.9343 3.7 ( 1 0 15) 15.219 0.1704 2.1413 30.602 2.9190 5.7 ( 0 2 14) 15.301 0.1713 2.1525 30.843 2.8967 3.7 ( 1-2 3) 15.422 0.1726 2.1691 31.774 2.8139 0.1 ( 0-1 5) 15.887 0.1777 2.2329 32.274 2.7714 0.1 ( 1 1 18) 16.137 0.1804 2.2672 32.475 2.7547 0.1 ( 2-1 9) 16.238 0.1815 2.2809 33.072 2.7064 0.1 ( 1 1 4) 16.536 0.1847 2.3216 33.072 2.7064 0.1 ( 2-1 7) 16.536 0.1847 2.3216 33.764 2.6525 1.5 (-1 2 9) 16.882 0.1885 2.3688 33.886 2.6432 4.1 ( 0 2 2) 16.943 0.1892 2.3771 34.206 2.6192 24.1 ( 2 0 14) 17.103 0.1909 2.3989 34.206 2.6192 24.1 ( 0 2 16) 17.103 0.1909 2.3989 34.518 2.5962 4.6 ( 2 0 12) 17.259 0.1926 2.4201 34.518 2.5962 4.6 ( 1-2 5) 17.259 0.1926 2.4201 35.100 2.5545 30.5 ( 2 0 16) 17.550 0.1957 2.4596 35.821 2.5047 38.9 ( 2 0 10) 17.910 0.1996 2.5085 35.821 2.5047 38.9 ( 1 0 17) 17.910 0.1996 2.5085 35.894 2.4998 26.1 ( 1 2 15) 17.947 0.2000 2.5135 36.079 2.4874 35.4 ( 2-2 4) 18.040 0.2010 2.5260 36.079 2.4874 35.4 ( 1 2 17) 18.040 0.2010 2.5260 36.653 2.4497 0.6 ( 1 1 20) 18.327 0.2041 2.5648 36.783 2.4414 1.1 ( 0 0 12) 18.391 0.2048 2.5736 36.783 2.4414 1.1 ( 1 2 13) 18.391 0.2048 2.5736 37.001 2.4275 9.1 ( 2 0 18) 18.500 0.2060 2.5883 37.323 2.4073 1.1 ( 1 2 19) 18.662 0.2077 2.6101 37.436 2.4003 0.8 ( 2-1 15) 18.718 0.2083 2.6177 37.617 2.3891 1.6 ( 0-1 7) 18.809 0.2093 2.6299 37.617 2.3891 1.6 ( 2-2 8) 18.809 0.2093 2.6299 38.163 2.3563 14.1 ( 0 2 0) 19.081 0.2122 2.6666 38.242 2.3516 8.9 (-1 3 8) 19.121 0.2126 2.6719 38.242 2.3516 8.9 ( 2 0 8) 19.121 0.2126 2.6719 38.534 2.3344 16.7 ( 0 2 18) 19.267 0.2142 2.6916 38.681 2.3259 10.2 ( 1 2 11) 19.340 0.2150 2.7014 38.763 2.3211 9.9 (-2 2 0) 19.382 0.2154 2.7070 39.542 2.2772 0.8 ( 1 2 21) 19.771 0.2196 2.7592 39.871 2.2591 1.9 ( 0 3 13) 19.936 0.2213 2.7813 39.871 2.2591 1.9 ( 2-2 10) 19.936 0.2213 2.7813 40.020 2.2511 1.4 (-1 0 5) 20.010 0.2221 2.7912 40.230 2.2398 0.6 ( 0 3 15) 20.115 0.2232 2.8052 40.379 2.2319 0.5 ( 1-1 14) 20.189 0.2240 2.8152 40.769 2.2114 16.4 ( 2 1 19) 20.385 0.2261 2.8413 40.769 2.2114 16.4 ( 2 1 17) 20.385 0.2261 2.8413 40.867 2.2064 25.4 ( 0 1 17) 20.433 0.2266 2.8478 40.945 2.2023 24.1 ( 2-1 1) 20.473 0.2270 2.8530 40.945 2.2023 24.1 ( 2-1 17) 20.473 0.2270 2.8530 41.502 2.1741 14.6 ( 0 3 17) 20.751 0.2300 2.8901 41.502 2.1741 14.6 ( 1 0 19) 20.751 0.2300 2.8901 41.588 2.1698 8.5 (-1 3 12) 20.794 0.2304 2.8958 41.588 2.1698 8.5 ( 1 1 22) 20.794 0.2304 2.8958 42.621 2.1195 8.2 ( 1 1 0) 21.310 0.2359 2.9644 42.621 2.1195 8.2 ( 1 2 23) 21.310 0.2359 2.9644 42.964 2.1034 2.8 ( 2-2 12) 21.482 0.2377 2.9872 42.964 2.1034 2.8 ( 0-2 2) 21.482 0.2377 2.9872 43.403 2.0831 9.2 ( 0 2 20) 21.701 0.2400 3.0162 43.403 2.0831 9.2 (-1 3 0) 21.701 0.2400 3.0162 43.549 2.0765 5.2 ( 2 1 13) 21.774 0.2408 3.0259 43.901 2.0606 2.2 (-2 3 1) 21.951 0.2426 3.0491 43.901 2.0606 2.2 ( 2-3 1) 21.951 0.2426 3.0491 44.553 2.0320 0.1 (-1 3 14) 22.277 0.2461 3.0922 44.707 2.0254 0.1 ( 2-3 3) 22.353 0.2469 3.1023 44.707 2.0254 0.1 ( 0 3 7) 22.353 0.2469 3.1023 45.004 2.0127 0.2 ( 1 2 7) 22.502 0.2484 3.1218 45.004 2.0127 0.2 (-2 2 4) 22.502 0.2484 3.1218 45.204 2.0042 1.9 (-2 1 1) 22.602 0.2495 3.1350 45.370 1.9973 1.2 ( 2 0 4) 22.685 0.2503 3.1459 45.955 1.9732 0.5 (-1 0 7) 22.978 0.2534 3.1843 46.387 1.9558 0.1 ( 2 1 25) 23.194 0.2556 3.2126 46.387 1.9558 0.1 ( 1 2 25) 23.194 0.2556 3.2126 46.499 1.9514 0.1 ( 2-3 5) 23.249 0.2562 3.2199 46.765 1.9409 1.7 ( 2-2 14) 23.382 0.2576 3.2373 46.765 1.9409 1.7 ( 1-3 2) 23.382 0.2576 3.2373 47.658 1.9066 0.1 ( 2 0 24) 23.829 0.2622 3.2955 48.081 1.8908 0.9 (-1 2 15) 24.041 0.2644 3.3230 48.081 1.8908 0.9 (-1-1 2) 24.041 0.2644 3.3230 48.220 1.8857 0.5 (-1 3 16) 24.110 0.2652 3.3321 48.300 1.8827 0.4 ( 0-2 4) 24.150 0.2656 3.3373 48.744 1.8666 0.8 ( 1 3 20) 24.372 0.2679 3.3661 48.744 1.8666 0.8 ( 0 2 22) 24.372 0.2679 3.3661 49.077 1.8547 0.5 ( 1-2 11) 24.538 0.2696 3.3876 49.077 1.8547 0.5 ( 1 3 22) 24.538 0.2696 3.3876 49.150 1.8521 0.4 ( 1 2 5) 24.575 0.2700 3.3924 49.150 1.8521 0.4 (-2 2 6) 24.575 0.2700 3.3924 49.812 1.8291 2.2 ( 0 0 16) 24.906 0.2734 3.4352 49.812 1.8291 2.2 ( 2 0 2) 24.906 0.2734 3.4352 49.986 1.8231 1.4 ( 0-1 11) 24.993 0.2743 3.4464 49.986 1.8231 1.4 (-2 1 3) 24.993 0.2743 3.4464 50.606 1.8022 0.1 ( 3-2 11) 25.303 0.2774 3.4864 50.606 1.8022 0.1 ( 2 2 24) 25.303 0.2774 3.4864 50.768 1.7969 0.2 ( 1 2 27) 25.384 0.2783 3.4968 51.162 1.7839 5.7 ( 3-2 9) 25.581 0.2803 3.5221 51.162 1.7839 5.7 ( 2-2 16) 25.581 0.2803 3.5221 51.563 1.7710 0.6 (-1 4 9) 25.782 0.2823 3.5478 52.154 1.7523 0.4 (-1 0 9) 26.077 0.2853 3.5857 52.294 1.7480 0.8 ( 2 2 18) 26.147 0.2860 3.5946 52.294 1.7480 0.8 ( 2-3 9) 26.147 0.2860 3.5946 52.509 1.7413 1.2 (-1 3 18) 26.254 0.2871 3.6083 52.509 1.7413 1.2 ( 3 0 19) 26.254 0.2871 3.6083 52.649 1.7370 0.8 ( 1 1 26) 26.325 0.2879 3.6173 52.649 1.7370 0.8 (-1 4 15) 26.325 0.2879 3.6173 52.809 1.7321 0.8 (-1 4 7) 26.405 0.2887 3.6275 52.937 1.7282 0.6 ( 3-1 10) 26.468 0.2893 3.6356 53.391 1.7146 19.9 ( 3 0 17) 26.695 0.2916 3.6645 53.495 1.7115 11.7 ( 2 2 28) 26.747 0.2921 3.6711 53.495 1.7115 11.7 ( 3-1 22) 26.747 0.2921 3.6711 53.737 1.7044 25.7 (-1 2 17) 26.869 0.2934 3.6865 53.865 1.7006 36.0 ( 3-2 17) 26.932 0.2940 3.6946 53.865 1.7006 36.0 (-2 2 8) 26.932 0.2940 3.6946 53.979 1.6973 14.9 ( 0-2 6) 26.989 0.2946 3.7019 54.132 1.6929 4.8 ( 0 4 18) 27.066 0.2954 3.7116 54.429 1.6843 33.5 ( 0 4 16) 27.215 0.2969 3.7304 54.429 1.6843 33.5 ( 2 2 16) 27.215 0.2969 3.7304 54.582 1.6800 41.2 ( 3 0 25) 27.291 0.2976 3.7401 54.582 1.6800 41.2 (-1 4 17) 27.291 0.2976 3.7401 54.879 1.6716 22.1 (-2 4 2) 27.439 0.2991 3.7588 54.879 1.6716 22.1 ( 2 0 0) 27.439 0.2991 3.7588 55.041 1.6670 13.4 ( 2-1 23) 27.520 0.2999 3.7691 55.041 1.6670 13.4 ( 3 0 15) 27.520 0.2999 3.7691 55.561 1.6527 0.8 (-2 4 8) 27.780 0.3025 3.8018 55.561 1.6527 0.8 ( 0 4 14) 27.780 0.3025 3.8018 55.663 1.6499 0.9 ( 1 2 29) 27.831 0.3031 3.8083 55.808 1.6459 1.1 ( 0 4 22) 27.904 0.3038 3.8174 56.071 1.6388 13.8 ( 3-3 4) 28.035 0.3051 3.8339 56.071 1.6388 13.8 ( 2-2 18) 28.035 0.3051 3.8339 56.172 1.6361 27.9 (-2 4 0) 28.086 0.3056 3.8403 56.172 1.6361 27.9 ( 2-3 11) 28.086 0.3056 3.8403 56.328 1.6320 14.5 ( 3-1 24) 28.164 0.3064 3.8501 56.328 1.6320 14.5 ( 0 3 1) 28.164 0.3064 3.8501 56.559 1.6258 15.3 ( 0 0 18) 28.279 0.3075 3.8646 56.559 1.6258 15.3 (-2 3 11) 28.279 0.3075 3.8646 57.268 1.6074 0.8 (-1 3 20) 28.634 0.3111 3.9089 57.268 1.6074 0.8 ( 2 2 14) 28.634 0.3111 3.9089 57.415 1.6036 1.2 ( 3 0 13) 28.708 0.3118 3.9182 57.415 1.6036 1.2 ( 0 4 12) 28.708 0.3118 3.9182 57.531 1.6007 0.6 (-1 4 3) 28.765 0.3124 3.9253 57.531 1.6007 0.6 ( 3-3 2) 28.765 0.3124 3.9253 57.673 1.5970 0.3 ( 2 0 28) 28.837 0.3131 3.9342 57.767 1.5947 0.4 ( 0 4 24) 28.884 0.3135 3.9401 58.199 1.5839 0.5 ( 2 1 5) 29.099 0.3157 3.9670 58.199 1.5839 0.5 ( 2-4 2) 29.099 0.3157 3.9670 58.350 1.5801 0.3 ( 1 3 30) 29.175 0.3164 3.9763 58.616 1.5736 0.2 (-1 0 11) 29.308 0.3177 3.9929 58.616 1.5736 0.2 ( 3 1 24) 29.308 0.3177 3.9929 58.788 1.5694 0.1 ( 1 3 10) 29.394 0.3186 4.0036 58.788 1.5694 0.1 ( 1 1 28) 29.394 0.3186 4.0036 59.010 1.5640 0.1 (-2 2 10) 29.505 0.3197 4.0173 59.295 1.5572 0.3 ( 2 2 32) 29.648 0.3211 4.0350 59.295 1.5572 0.3 ( 0 3 27) 29.648 0.3211 4.0350 59.750 1.5464 1.0 ( 3 0 29) 29.875 0.3233 4.0631 59.750 1.5464 1.0 (-1 2 19) 29.875 0.3233 4.0631 59.946 1.5418 0.6 ( 0 4 10) 29.973 0.3243 4.0752 59.946 1.5418 0.6 (-2 4 12) 29.973 0.3243 4.0752 60.326 1.5330 3.0 (-2 0 2) 30.163 0.3262 4.0986 60.326 1.5330 3.0 ( 1 0 25) 30.163 0.3262 4.0986 60.462 1.5299 2.0 (-1 4 21) 30.231 0.3268 4.1069 60.462 1.5299 2.0 ( 3 0 11) 30.231 0.3268 4.1069 60.712 1.5242 0.5 ( 2 2 12) 30.356 0.3280 4.1223 60.712 1.5242 0.5 (-1 1 16) 30.356 0.3280 4.1223 60.871 1.5206 1.6 ( 1-2 15) 30.436 0.3288 4.1321 60.871 1.5206 1.6 (-1 4 1) 30.436 0.3288 4.1321 61.015 1.5173 1.3 (-2 3 13) 30.508 0.3295 4.1409 61.015 1.5173 1.3 ( 1 2 31) 30.508 0.3295 4.1409 61.202 1.5132 0.4 ( 3 1 30) 30.601 0.3304 4.1524 61.437 1.5079 0.2 ( 2-2 20) 30.719 0.3316 4.1668 62.660 1.4814 0.4 ( 2 3 29) 31.330 0.3375 4.2414 62.660 1.4814 0.4 ( 3 1 18) 31.330 0.3375 4.2414 63.138 1.4713 22.1 ( 3-4 3) 31.569 0.3398 4.2704 63.138 1.4713 22.1 ( 2 2 34) 31.569 0.3398 4.2704 63.308 1.4678 14.6 ( 2 0 30) 31.654 0.3406 4.2807 63.308 1.4678 14.6 ( 3-4 1) 31.654 0.3406 4.2807 |
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13659058978 2026-03-24 | 4/200 |
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