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藍(lán)色悠云金蟲 (小有名氣)
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[求助]
求助幾個B類錯誤。。! 已有3人參與
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Alert level B CHEMS01_ALERT_1_B The sum formula contains elements in the wrong order. H precedes Cu Sequence must be alphabetical for inorganic structures. PLAT043_ALERT_1_B Calculated and Reported Mol. Weight Differ by .. 27.29 Check PLAT051_ALERT_1_B Mu(calc) and Mu(CIF) Ratio Differs from 1.0 by . 7.33 % PLAT391_ALERT_3_B Deviating Methyl C2 H-C-H Bond Angle ...... 99 Degree |
用戶注銷 (知名作家)
精修問題可私信
捐助貴賓 (著名寫手)
木蟲 (正式寫手)
金蟲 (小有名氣)
捐助貴賓 (著名寫手)
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數(shù)據(jù)已經(jīng)處理好,見附件。 Bond precision: C-C = 0.0041 A Wavelength=0.71073 Cell: a=7.5293(4) b=10.5098(7) c=10.7922(6) alpha=76.518(5) beta=81.175(4) gamma=79.695(5) Temperature: 293 K Calculated Reported Volume 811.48(9) 811.48(8) Space group P -1 P-1 Hall group -P 1 ? Moiety formula C36 H32 Cu N6 O4 S2 ? Sum formula C36 H32 Cu N6 O4 S2 C36 H32 Cu N6 O4 S2 Mr 740.35 740.35 Dx,g cm-3 1.515 1.515 Z 1 1 Mu (mm-1) 0.853 0.853 F000 383.0 383.0 F000' 383.69 h,k,lmax 9,12,12 9,12,12 Nref 2959 2951 Tmin,Tmax 0.829,0.858 0.835,0.862 Tmin' 0.829 Correction method= # Reported T Limits: Tmin=0.835 Tmax=0.862 AbsCorr = MULTI-SCAN Data completeness= 0.997 Theta(max)= 25.350 R(reflections)= 0.0367( 2437) wR2(reflections)= 0.0944( 2951) S = 1.026 Npar= 272 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT420_ALERT_2_C D-H Without Acceptor N1 - H1N .. Please Check Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! |
金蟲 (小有名氣)
送紅花一朵 |
可不可以幫我把這幾個錯誤也改一下呢?需要數(shù)據(jù)的話我上傳~ DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. SHFSU01_ALERT_2_A The absolute value of parameter shift to su ratio > 0.20 Absolute value of the parameter shift to su ratio given 1.384 Additional refinement cycles may be required. PLAT080_ALERT_2_A Maximum Shift/Error ............................ 1.38 Why ? PLAT223_ALERT_4_A Large Solvent/Anion H Ueq(max)/Ueq(min) ..... 5.3 Ratio PLAT415_ALERT_2_A Short Inter D-H..H-X H23A .. H43 .. 1.58 Ang. Alert level B PLAT222_ALERT_3_B Large Non-Solvent H Uiso(max)/Uiso(min) ... 7.5 Ratio PLAT420_ALERT_2_B D-H Without Acceptor O14 - H14A .. Please Check |
捐助貴賓 (著名寫手)
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