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ylt木蟲(chóng) (著名寫(xiě)手)
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[求助]
A,B類(lèi)錯(cuò)誤,希望大家?guī)蛶臀医鉀Q一下,至少能解決掉A類(lèi) 已有4人參與
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SYMM001_ALERT_1_A _symmetry_cell_setting is missing The cell setting should be one of the following * triclinic * monoclinic * orthorhombic * tetragonal * rhombohedral * trigonal * hexagonal * cubic The following tests will not be performed. SYMMS_01,SYMMS_02 EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 RINTA01_ALERT_3_A The value of Rint is greater than 0.25 Rint given 0.329 SHFSU01_ALERT_2_A The absolute value of parameter shift to su ratio > 0.20 Absolute value of the parameter shift to su ratio given 0.815 Additional refinement cycles may be required. PLAT020_ALERT_3_A The value of Rint is greater than 0.12 ......... 0.329 Report PLAT075_ALERT_1_A Occupancy 2. greater than 1.0 for ...... O15 PLAT080_ALERT_2_A Maximum Shift/Error ............................ 0.81 PLAT122_ALERT_1_A No _symmetry_space_group_name_H-M Given ........ Please Do ! PLAT430_ALERT_2_A Short Inter D...A Contact O16 .. O16 .. 1.81 Ang. PLAT430_ALERT_2_A Short Inter D...A Contact O16 .. O16 .. 1.81 Ang. CHEMS01_ALERT_1_B The sum formula contains elements in the wrong order. H precedes Cu Sequence must be alphabetical for inorganic structures. PLAT043_ALERT_1_B Calculated and Reported Mol. Weight Differ by .. 14.62 Check PLAT057_ALERT_3_B Correction for Absorption Required RT(exp) ... 1.25 Do ! PLAT306_ALERT_2_B Isolated Oxygen Atom (H-atoms Missing ?) ....... O16 Check PLAT341_ALERT_3_B Low Bond Precision on C-C Bonds ............... 0.0160 Ang. PLAT430_ALERT_2_B Short Inter D...A Contact O18 .. O18 .. 2.80 Ang. PLAT430_ALERT_2_B Short Inter D...A Contact O18 .. O18 .. 2.80 Ang. PLAT601_ALERT_2_B Structure Contains Solvent Accessible VOIDS of . 151 Ang3 |
晶體結(jié)構(gòu)解析 |

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R值太高了,可能沒(méi)解完,也可能數(shù)據(jù)不好,能解決到什么程度取決于數(shù)據(jù)的好壞 [ 發(fā)自小木蟲(chóng)客戶(hù)端 ] |

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