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cedar421126金蟲 (小有名氣)
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[求助]
求助幫忙解析一個(gè)晶體,求各位大俠幫忙跪求 已有3人參與
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| 求解析一個(gè)晶體,各位大俠幫幫忙 謝謝了! 小弟幣子不多100奉上 謝謝 |
捐助貴賓 (著名寫手)
金蟲 (小有名氣)
木蟲 (正式寫手)
專家顧問 (文壇精英)
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專家經(jīng)驗(yàn): +1066 |

捐助貴賓 (著名寫手)
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數(shù)據(jù)見附件。 Bond precision: C-C = 0.0083 A Wavelength=0.71073 Cell: a=15.4128(12) b=15.4162(12) c=41.620(3) alpha=90 beta=100.789(2) gamma=90 Temperature: 293 K Calculated Reported Volume 9714.4(13) 9714.4(13) Space group P 21/c P21/c Hall group -P 2ybc ? Moiety formula C20 H30 Cl4 O Ti2 ? Sum formula C20 H30 Cl4 O Ti2 C20 H30 Cl4 O Ti2 Mr 523.98 523.98 Dx,g cm-3 1.433 1.433 Z 16 16 Mu (mm-1) 1.106 1.106 F000 4320.0 4320.0 F000' 4339.33 h,k,lmax 19,19,51 19,19,51 Nref 19177 19091 Tmin,Tmax 0.784,0.819 0.793,0.826 Tmin' 0.784 Correction method= # Reported T Limits: Tmin=0.793 Tmax=0.826 AbsCorr = MULTI-SCAN Data completeness= 0.996 Theta(max)= 26.060 R(reflections)= 0.0640( 9447) wR2(reflections)= 0.1577( 19091) S = 0.983 Npar= 1013 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 49 % PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0083 Ang. |
木蟲 (正式寫手)
木蟲 (正式寫手)
商家已經(jīng)主動(dòng)聲明此回帖可能含有宣傳內(nèi)容|
Bond precision: C-C = 0.0049 A Wavelength=0.71073 Cell: a=15.4128(12) b=15.4162(12) c=41.620(3) alpha=90 beta=100.789(2) gamma=90 Temperature: 293 K Calculated Reported Volume 9714.4(13) 9714.4(13) Space group P 21/c P21/c Hall group -P 2ybc ? Moiety formula C20 H30 Cl4 O Ti2 ? Sum formula C20 H30 Cl4 O Ti2 C20 H30 Cl4 O Ti2 Mr 523.98 523.98 Dx,g cm-3 1.433 1.433 Z 16 16 Mu (mm-1) 1.106 1.106 F000 4320.0 4320.0 F000' 4339.33 h,k,lmax 18,18,49 18,18,49 Nref 17125 17080 Tmin,Tmax 0.784,0.819 0.793,0.826 Tmin' 0.784 Correction method= # Reported T Limits: Tmin=0.793 Tmax=0.826 AbsCorr = MULTI-SCAN Data completeness= 0.997 Theta(max)= 25.010 R(reflections)= 0.0587( 8744) wR2(reflections)= 0.1273( 17080) S = 1.050 Npar= 1013 -------------------------------------------------------------------------------- The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. --------------------------------------------------------------------------------Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 6 Report PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! |
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