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[求助]
求助一個關(guān)于加H限制精修的審稿問題
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Please check the H restraints definitions in Experimental (they would be in the SHELXL file if it had been submitted). It would be helpful to include the final SHELXL input files within the CIF (under a _iucr_refine_instruction_details section. [ Last edited by hcht2006 on 2011-5-25 at 09:42 ] |

至尊木蟲 (著名寫手)

鐵桿木蟲 (著名寫手)

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Carbon-bound H atoms were positioned geometrically (C–H=0.93Å and refined as riding atoms, with Uiso(H) values fixed at 1.2Ueq(C). The water H atom was located in a difference Fourier map and included in the subsequent refinement using the restraints O–H=0.85Å and H···H=1.39Å. In the last cycles of refinement, they were treated as riding on the O atoms to which they are attached, with Uiso(H)=–1.5Ueq(O).正文當(dāng)中是這樣寫的,請問CIF中應(yīng)該如何寫,謝謝 |

至尊木蟲 (著名寫手)
至尊木蟲 (著名寫手)
銀蟲 (正式寫手)
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