| 3 | 1/1 | 返回列表 |
| 查看: 892 | 回復(fù): 2 | |||
阿木100木蟲 (正式寫手)
|
[求助]
XPS校正方法 英文書寫(參考文獻(xiàn))
|
|
審稿人提問說,能量校正的方法應(yīng)該給出 The method of binding energy calibration in XPS spectra should be detailed. 問了測試?yán)蠋熓沁@樣說的:用Ni樣品做費(fèi)米能級(jí)校正,分別用Cu、Ag、Au三種元素做能量校準(zhǔn),用污染碳C 284.6eV作核電位移校正。 求英文翻譯,或者參考文獻(xiàn) 能提供參考文獻(xiàn)就可以了,只要文獻(xiàn)有寫這些條件就OK了,實(shí)在是不會(huì)翻譯 |
至尊木蟲 (文壇精英)
|
XPS analyseswere performed with a V.G. Scientific ESCALAB250 using focused (diameter of the irradiated area was approximately 500m) monochromated Al K (h = 1486.6 eV, 150W). An electron shower was used in order to compensate for charging effects. Ahemispherical electrostatic analyzer and a LargeAreaXL Lenswere used tomaximize the signal. The residual pressure inside the analysis chamber was 6×10−10 mbar. The spectrometer was calibrated using the photoemission lines of Au (Au 4f7/2 = 83.95 eV), Ag (Ag 3d5/2 = 368.22 eV) and Cu (Cu 2p3/2 = 932.62 eV). The peaks were recorded at a constant pass energy of 20 eV and XPS datawere taken at normal emission ( =0◦ for all catalysts. No smoothing routineof data was applied to the data during the analysis. Atomic ratios were then computed from the intensity ratios normalized by the atomic sensitivity factors of Scofield [6]. A Shirley-type background subtraction was done prior to curve fitting, and fitting the experimental curve to 80% Gaussian–20% Lorentzian function. In addition, aminimum number of doubletswere always used in order to fit the experimental curves. W. Huang et al. / Journal of Electron Spectroscopy and Related Phenomena 173 (2009) 88–95 |
木蟲 (正式寫手)

| 3 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 384求調(diào)劑 +3 | 子系博 2026-03-22 | 6/300 |
|
|---|---|---|---|---|
|
[考研] 一志愿重慶大學(xué)085700資源與環(huán)境,總分308求調(diào)劑 +7 | 墨墨漠 2026-03-23 | 8/400 |
|
|
[考研] 0854電子信息求調(diào)劑 324 +3 | Promise-jyl 2026-03-23 | 3/150 |
|
|
[考研] 一志愿 西北大學(xué) ,070300化學(xué)學(xué)碩,總分287,雙非一本,求調(diào)劑。 +3 | 晨昏線與星海 2026-03-20 | 3/150 |
|
|
[考研] 生物學(xué)調(diào)劑 +5 | Surekei 2026-03-21 | 5/250 |
|
|
[基金申請(qǐng)] 山東省面上項(xiàng)目限額評(píng)審 +4 | 石瑞0426 2026-03-19 | 4/200 |
|
|
[考研] 286求調(diào)劑 +10 | Faune 2026-03-21 | 10/500 |
|
|
[考研] 0805 316求調(diào)劑 +3 | 大雪深藏 2026-03-18 | 3/150 |
|
|
[考研] 0703化學(xué)調(diào)劑 +4 | 妮妮ninicgb 2026-03-21 | 4/200 |
|
|
[考研] 一志愿深大,0703化學(xué),總分302,求調(diào)劑 +4 | 七月-七七 2026-03-21 | 4/200 |
|
|
[考研] 265求調(diào)劑 +12 | 梁梁校校 2026-03-19 | 14/700 |
|
|
[考研] 332求調(diào)劑 +4 | ydfyh 2026-03-17 | 4/200 |
|
|
[考研] 一志愿華南師大 070300(化學(xué))304分求調(diào)劑 +3 | 0703武芊慧雪304 2026-03-18 | 3/150 |
|
|
[考研] 294求調(diào)劑材料與化工專碩 +15 | 陌の森林 2026-03-18 | 15/750 |
|
|
[考研] 考研調(diào)劑求學(xué)校推薦 +3 | 伯樂29 2026-03-18 | 5/250 |
|
|
[考研] A區(qū)線材料學(xué)調(diào)劑 +5 | 周周無極 2026-03-20 | 5/250 |
|
|
[考研] 295材料求調(diào)劑,一志愿武漢理工085601專碩 +5 | Charlieyq 2026-03-19 | 5/250 |
|
|
[考研] 材料學(xué)碩318求調(diào)劑 +5 | February_Feb 2026-03-19 | 5/250 |
|
|
[考研] 一志愿中國海洋大學(xué),生物學(xué),301分,求調(diào)劑 +5 | 1孫悟空 2026-03-17 | 6/300 |
|
|
[考研] 材料,紡織,生物(0856、0710),化學(xué)招生啦 +3 | Eember. 2026-03-17 | 9/450 |
|