| 5 | 1/1 | 返回列表 |
| 查看: 891 | 回復(fù): 2 | ||
| 當(dāng)前只顯示滿足指定條件的回帖,點擊這里查看本話題的所有回帖 | ||
阿木100木蟲 (正式寫手)
|
[求助]
XPS校正方法 英文書寫(參考文獻)
|
|
|
審稿人提問說,能量校正的方法應(yīng)該給出 The method of binding energy calibration in XPS spectra should be detailed. 問了測試?yán)蠋熓沁@樣說的:用Ni樣品做費米能級校正,分別用Cu、Ag、Au三種元素做能量校準(zhǔn),用污染碳C 284.6eV作核電位移校正。 求英文翻譯,或者參考文獻 能提供參考文獻就可以了,只要文獻有寫這些條件就OK了,實在是不會翻譯 |
木蟲 (正式寫手)

至尊木蟲 (文壇精英)
|
XPS analyseswere performed with a V.G. Scientific ESCALAB250 using focused (diameter of the irradiated area was approximately 500m) monochromated Al K (h = 1486.6 eV, 150W). An electron shower was used in order to compensate for charging effects. Ahemispherical electrostatic analyzer and a LargeAreaXL Lenswere used tomaximize the signal. The residual pressure inside the analysis chamber was 6×10−10 mbar. The spectrometer was calibrated using the photoemission lines of Au (Au 4f7/2 = 83.95 eV), Ag (Ag 3d5/2 = 368.22 eV) and Cu (Cu 2p3/2 = 932.62 eV). The peaks were recorded at a constant pass energy of 20 eV and XPS datawere taken at normal emission ( =0◦ for all catalysts. No smoothing routineof data was applied to the data during the analysis. Atomic ratios were then computed from the intensity ratios normalized by the atomic sensitivity factors of Scofield [6]. A Shirley-type background subtraction was done prior to curve fitting, and fitting the experimental curve to 80% Gaussian–20% Lorentzian function. In addition, aminimum number of doubletswere always used in order to fit the experimental curves. W. Huang et al. / Journal of Electron Spectroscopy and Related Phenomena 173 (2009) 88–95 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 材料調(diào)劑 +3 | 匹克i 2026-03-23 | 3/150 |
|
|---|---|---|---|---|
|
[考研] 一志愿重慶大學(xué)085700資源與環(huán)境,總分308求調(diào)劑 +7 | 墨墨漠 2026-03-23 | 8/400 |
|
|
[考研] 336求調(diào)劑 +4 | 收到VS 2026-03-20 | 4/200 |
|
|
[考研]
|
孅華 2026-03-22 | 4/200 |
|
|
[考研] 工科材料085601 279求調(diào)劑 +8 | 困于星晨 2026-03-17 | 10/500 |
|
|
[考研] 276求調(diào)劑 +3 | YNRYG 2026-03-21 | 4/200 |
|
|
[考研] 一志愿華中科技大學(xué)071000,求調(diào)劑 +4 | 沿岸有貝殼6 2026-03-21 | 4/200 |
|
|
[考研] 280求調(diào)劑 +11 | 咕嚕曉曉 2026-03-18 | 12/600 |
|
|
[考研] 一志愿南大,0703化學(xué),分?jǐn)?shù)336,求調(diào)劑 +3 | 收到VS 2026-03-21 | 3/150 |
|
|
[考研] 材料學(xué)學(xué)碩080502 337求調(diào)劑-一志愿華中科技大學(xué) +4 | 順順順mr 2026-03-18 | 5/250 |
|
|
[考研] 材料工程(專)一志愿985 初試335求調(diào)劑 +3 | hiloiy 2026-03-17 | 4/200 |
|
|
[考研] 華東師范大學(xué)-071000生物學(xué)-293分-求調(diào)劑 +3 | 研究生何瑤明 2026-03-18 | 3/150 |
|
|
[考研] 一志愿南昌大學(xué),327分,材料與化工085600 +9 | Ncdx123456 2026-03-19 | 9/450 |
|
|
[考研] 321求調(diào)劑 +9 | 何潤采123 2026-03-18 | 11/550 |
|
|
[考研] 求調(diào)劑一志愿南京航空航天大學(xué)289分 +3 | @taotao 2026-03-19 | 3/150 |
|
|
[考研] A區(qū)線材料學(xué)調(diào)劑 +5 | 周周無極 2026-03-20 | 5/250 |
|
|
[考研] 材料學(xué)碩297已過四六級求調(diào)劑推薦 +11 | adaie 2026-03-19 | 11/550 |
|
|
[考研] 0817 化學(xué)工程 299分求調(diào)劑 有科研經(jīng)歷 有二區(qū)文章 +22 | rare12345 2026-03-18 | 22/1100 |
|
|
[考研] 一志愿西安交通大學(xué) 學(xué)碩 354求調(diào)劑211或者雙一流 +3 | 我想要讀研究生 2026-03-20 | 3/150 |
|
|
[考研] 考研求調(diào)劑 +3 | 橘頌. 2026-03-17 | 4/200 |
|