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阿木100木蟲 (正式寫手)
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[求助]
XPS校正方法 英文書寫(參考文獻(xiàn))
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審稿人提問說,能量校正的方法應(yīng)該給出 The method of binding energy calibration in XPS spectra should be detailed. 問了測試?yán)蠋熓沁@樣說的:用Ni樣品做費(fèi)米能級校正,分別用Cu、Ag、Au三種元素做能量校準(zhǔn),用污染碳C 284.6eV作核電位移校正。 求英文翻譯,或者參考文獻(xiàn) 能提供參考文獻(xiàn)就可以了,只要文獻(xiàn)有寫這些條件就OK了,實(shí)在是不會翻譯 |
至尊木蟲 (文壇精英)
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XPS analyseswere performed with a V.G. Scientific ESCALAB250 using focused (diameter of the irradiated area was approximately 500m) monochromated Al K (h = 1486.6 eV, 150W). An electron shower was used in order to compensate for charging effects. Ahemispherical electrostatic analyzer and a LargeAreaXL Lenswere used tomaximize the signal. The residual pressure inside the analysis chamber was 6×10−10 mbar. The spectrometer was calibrated using the photoemission lines of Au (Au 4f7/2 = 83.95 eV), Ag (Ag 3d5/2 = 368.22 eV) and Cu (Cu 2p3/2 = 932.62 eV). The peaks were recorded at a constant pass energy of 20 eV and XPS datawere taken at normal emission ( =0◦ for all catalysts. No smoothing routineof data was applied to the data during the analysis. Atomic ratios were then computed from the intensity ratios normalized by the atomic sensitivity factors of Scofield [6]. A Shirley-type background subtraction was done prior to curve fitting, and fitting the experimental curve to 80% Gaussian–20% Lorentzian function. In addition, aminimum number of doubletswere always used in order to fit the experimental curves. W. Huang et al. / Journal of Electron Spectroscopy and Related Phenomena 173 (2009) 88–95 |
木蟲 (正式寫手)

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