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[求助]
100金幣在線急求助BC類錯(cuò)誤處理! 已有1人參與
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數(shù)據(jù)報(bào)的錯(cuò)誤應(yīng)該比較常見,即: Alert level B PLAT919_ALERT_3_B Reflection # Likely Affected by the Beamstop ... 1 Check #=============================================================================== Alert level C PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 Note PLAT934_ALERT_3_C Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 1 Check 如那位熱心朋友能幫忙處理一下,請(qǐng)及時(shí)聯(lián)系呀,在線急等,謝謝了! |
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The data set should be modified. There is one reflection that seems to be affected by the beamstop and 1 reflection shows a (Iobs-Icalc)/sigma w > 10. Both reflections should be identified and deleted using the OMIT instruction. In addition, the data set seems to have been merged because there are no negative intensities. The final refinement should be re-performed without the two reflections mentioned above and without merging the data. 審稿人提的這個(gè)問題,只要omit就可以了嗎, 請(qǐng)大家指點(diǎn)呀 |
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