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[求助]
求高人解析單晶 已有2人參與
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| 高人幫忙 |
捐助貴賓 (著名寫手)
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解析的結(jié)果見附件。 Bond precision: C-C = 0.0017 A Wavelength=0.71073 Cell: a=7.4900(15) b=11.800(2) c=8.0500(16) alpha=90 beta=110.15(3) gamma=90 Temperature: 293 K Calculated Reported Volume 667.9(3) 667.9(2) Space group P 21/c P2(1)/c Hall group -P 2ybc ? Moiety formula H O4 P, C2 H10 N2 ? Sum formula C2 H11 N2 O4 P C2 H11 N2 O4 P Mr 158.10 158.10 Dx,g cm-3 1.572 1.572 Z 4 4 Mu (mm-1) 0.365 0.365 F000 336.0 336.0 F000' 336.59 h,k,lmax 9,15,10 9,15,10 Nref 1538 1534 Tmin,Tmax 0.923,0.936 0.924,0.937 Tmin' 0.923 Correction method= # Reported T Limits: Tmin=0.924 Tmax=0.937 AbsCorr = MULTI-SCAN Data completeness= 0.997 Theta(max)= 27.480 R(reflections)= 0.0275( 1456) wR2(reflections)= 0.0856( 1534) S = 1.033 Npar= 111 The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT066_ALERT_1_G Predicted and Reported Tmin&Tmax Range Identical ? Check PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3 PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 6 Note |
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