| 24小時(shí)熱門(mén)版塊排行榜 |
| 8 | 1/1 | 返回列表 |
| 查看: 1195 | 回復(fù): 7 | |||||
lihuihui520新蟲(chóng) (小有名氣)
|
[求助]
如何對(duì)審稿人的問(wèn)題進(jìn)行合理解釋? 已有3人參與
|
|
晶體學(xué)數(shù)據(jù)問(wèn)題,求助高手幫忙分析,小女子萬(wàn)分感激: 1. We see from the CIF that there are 2 Uiso/Uij restrained atom sites, 3 distance or angle restraints and 15 least-squares restraints used in the refinement. So that the reader can be fully aware of what was done to generate the reported models, we should be told - at least in the "_refine_special_details" section of the CIF or in an ESI text - exactly what these restraints were and why they were necessary. [An easy way to show what restraints were employed (but not why they were needed) is to include the relevant lines from the SHELXL. ins file in the "_refine_special_details" section of the CIF. This should now be done.] 這是我在解決錯(cuò)誤時(shí),所加的命令: simu 0.01 0.02 3.8 $n simu 0.01 0.02 3.8 $c delu 0.002 C40 DFIX c39 n8 2.65 ISOR 0.001 c39 C40 dfix N8 C40 1.1 dfix C39 C40 1.4 2. Where there is crystallographically imposed symmetry in these structures we should be explicitly told about this in the appropriate descriptive text. 這個(gè)是在哪里能看到提議的對(duì)稱性? |
專家顧問(wèn) (文壇精英)
![]() |
專家經(jīng)驗(yàn): +1066 |
|
第一個(gè)問(wèn)題,你需要在CIF文件_refine_special_details 加上你的這些個(gè)限制性精修的命令,然后在ESI里面解釋為什么使用這些個(gè)命令 第二個(gè)關(guān)于結(jié)構(gòu)對(duì)稱性的問(wèn)題,這個(gè)需要具體結(jié)合結(jié)構(gòu)來(lái)看,比如某個(gè)原子處于二重軸,或者鏡面什么的 發(fā)自小木蟲(chóng)Android客戶端 |

用戶注銷(xiāo) (知名作家)
精修問(wèn)題可私信
鐵桿木蟲(chóng) (著名寫(xiě)手)
新蟲(chóng) (小有名氣)
新蟲(chóng) (小有名氣)
至尊木蟲(chóng) (著名寫(xiě)手)
新蟲(chóng) (小有名氣)
| 8 | 1/1 | 返回列表 |
| 最具人氣熱帖推薦 [查看全部] | 作者 | 回/看 | 最后發(fā)表 | |
|---|---|---|---|---|
|
[考研] 一志愿北京化工大學(xué)材料與化工(085600)296求調(diào)劑 +6 | 稻妻小編 2026-03-26 | 6/300 |
|
|---|---|---|---|---|
|
[考研] 297求調(diào)劑 +3 | 田洪有 2026-03-26 | 3/150 |
|
|
[考研] 考研一志愿蘇州大學(xué)初始315(英一)求調(diào)劑 +3 | sbdksD 2026-03-24 | 4/200 |
|
|
[考研]
|
孅華 2026-03-22 | 9/450 |
|
|
[考研] 281求調(diào)劑 +4 | Koxui 2026-03-24 | 5/250 |
|
|
[考研] 材料調(diào)劑 +3 | iwinso 2026-03-23 | 3/150 |
|
|
[考研] 一志愿吉林大學(xué)材料與化工303分求調(diào)劑 +4 | 為學(xué)666 2026-03-24 | 4/200 |
|
|
[考研]
材料學(xué)碩,求調(diào)劑
6+4
|
糖葫蘆888ll 2026-03-22 | 9/450 |
|
|
[考研] 286求調(diào)劑 +11 | Faune 2026-03-21 | 11/550 |
|
|
[考研] 上海電力大學(xué)材料防護(hù)與新材料重點(diǎn)實(shí)驗(yàn)室招收調(diào)劑研究生(材料、化學(xué)、電化學(xué),環(huán)境) +4 | 我愛(ài)學(xué)電池 2026-03-23 | 4/200 |
|
|
[考研] 0703化學(xué)調(diào)劑,求導(dǎo)師收 +7 | 天天好運(yùn)來(lái)上岸?/a> 2026-03-24 | 7/350 |
|
|
[有機(jī)交流]
20+3
|
FENGSHUJEI 2026-03-23 | 5/250 |
|
|
[考研] 341求調(diào)劑(一志愿湖南大學(xué)070300) +5 | 番茄頭--- 2026-03-22 | 6/300 |
|
|
[考研] 一志愿武理材料工程348求調(diào)劑 +6 |  ̄^ ̄゜汗 2026-03-19 | 9/450 |
|
|
[考研] 一志愿中南化學(xué)(0703)總分337求調(diào)劑 +9 | niko- 2026-03-19 | 10/500 |
|
|
[考研] 生物學(xué)調(diào)劑 +5 | Surekei 2026-03-21 | 5/250 |
|
|
[考研] 一志愿南大,0703化學(xué),分?jǐn)?shù)336,求調(diào)劑 +3 | 收到VS 2026-03-21 | 3/150 |
|
|
[考研] 330求調(diào)劑0854 +3 | assdll 2026-03-21 | 3/150 |
|
|
[考研] 一志愿南理工085701環(huán)境302求調(diào)劑院校 +3 | 葵梓衛(wèi)隊(duì) 2026-03-20 | 3/150 |
|
|
[考研] 0856調(diào)劑,是學(xué)校就去 +8 | sllhht 2026-03-19 | 9/450 |
|